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Microstructure and morphology of amine-cured epoxy coatings before and after outdoor exposures - an AFM study / Xiaohong Gu in JOURNAL OF COATINGS TECHNOLOGY AND RESEARCH, Vol. 2, N° 7 (07/2005)
[article]
Titre : Microstructure and morphology of amine-cured epoxy coatings before and after outdoor exposures - an AFM study Type de document : texte imprimé Auteurs : Xiaohong Gu, Auteur ; Y. C. Jean, Auteur ; Derek L. Ho, Auteur ; Jonathan W. Martin, Auteur ; Eric Byrd, Auteur ; Li-Piin Sung, Auteur ; Aziz Rezig, Auteur ; Joan Jasmin, Auteur ; Bouchra Kidah, Auteur ; David Martin, Auteur ; Mounina Oudina, Auteur ; Tinh Nguyen, Auteur Année de publication : 2005 Article en page(s) : p. 547-556 Note générale : Bibliogr. Langues : Américain (ame) Tags : Dégradation photooxydante photochimique Propriété chimique Etude expérimentale Diffusion neutron centrale Microscopie force atomique Résistance intempérie Méthode analyse Durabilité Epoxyde résine Structure surface Temps exposition Relation mise en oeuvre propriété Amine Durcissement(matière plastique) Vieillissement produit Matériau revêtement Morphologie Microstructure Index. décimale : 667.9 Revêtements et enduits Résumé : Atomic force microscopy (AFM) has been used to study the morphology and microstructure of an amine-cured epoxy before and after outdoor exposure. Measurements were made from samples prepared in an essentially CO2-free, H2O-free glove box and from samples prepared in ambient conditions. For those prepared in a CO2-free glove box, AFM imaging was conducted on (1) an unexposed air/coating surface, (2) an unexposed coating bulk, (3) an unexposed coating/substrate interface, and (4) a field exposed air/coating surface. For samples prepared in ambient conditions, only the unexposed air/coating surface was investigated. The same regions of the exposed samples were scanned periodically by the AFM to monitor changes in the surface morphology of the coating as UV exposure progressed. Small angle neutron scattering and Fourier transfonn infrared spectroscopy (FTIR) studies were performed to verify the microstructure and to follow chemical changes during outdoor exposure, respectively. The results have shown that amine blushing, which occurs only under ambient conditions, had a significant effect on the surface morphology and microstructure of the epoxy. The surface morphology of the samples prepared under CO2-free, dry conditions was generally smooth and homogeneous. However, the interface and the bulk samples clearly revealed a two-phase structure consisting of bright nodular domains and dark interstitial regions, indicating an inhomogeneous microstructure. Such heterogeneous structure of the bulk was in good agreement with results obtained by small angle neutron scattering of unexposed samples and by AFM phase imaging of the degraded sample surface. The relationship between submicrometer physical changes and molecular chemical degradation is discussed. DOI : 10.1007/s11998-005-0014-x En ligne : https://link.springer.com/content/pdf/10.1007%2Fs11998-005-0014-x.pdf Format de la ressource électronique : Permalink : https://e-campus.itech.fr/pmb/opac_css/index.php?lvl=notice_display&id=3802
in JOURNAL OF COATINGS TECHNOLOGY AND RESEARCH > Vol. 2, N° 7 (07/2005) . - p. 547-556[article]Réservation
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Code-barres Cote Support Localisation Section Disponibilité 002327 - Périodique Bibliothèque principale Documentaires Disponible Structural analysis of coating film with ultra-small-angle X-ray scattering / Iwao Soga in JOURNAL OF COATINGS TECHNOLOGY (JCT), Vol. 73, N° 919 (08/2001)
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Titre : Structural analysis of coating film with ultra-small-angle X-ray scattering Type de document : texte imprimé Auteurs : Iwao Soga, Auteur ; Hideki Matsuoka, Auteur Année de publication : 2001 Article en page(s) : p. 105-110 Note générale : Bibliogr. Langues : Américain (ame) Tags : Matériau revêtement Peinture magnétique Analyse structurale Diffusion RX centrale Index. décimale : 667.9 Revêtements et enduits Résumé : The structure of magnetic coating films was analyzed by the ultra-small-angle X-ray scattering (USAXS) technique. Small-angle X-ray scattering (SAXS) has been used to investigate the size, shape, and correlation of the nm sized structure. USAXS, with a measurable range extending to the µm order, can be used to analyze the submicron sized structure of paints and coating films. Preliminary USAXS experiments for a magnetic paint and magnetic coating films revealed that USAXS is useful to evaluate the structure of the particles in the paint and the films. Combined with other experimental methods, USAXS will provide a new kind of information about the structural analysis. Permalink : https://e-campus.itech.fr/pmb/opac_css/index.php?lvl=notice_display&id=5744
in JOURNAL OF COATINGS TECHNOLOGY (JCT) > Vol. 73, N° 919 (08/2001) . - p. 105-110[article]Réservation
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Code-barres Cote Support Localisation Section Disponibilité 001227 - Périodique Bibliothèque principale Documentaires Disponible