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Synthesis and characterization of organosilicon-modified self-matting waterborne polyurethane with excellent wear resistance / Pengfei Niu in JOURNAL OF COATINGS TECHNOLOGY AND RESEARCH, Vol. 20, N° 6 (11/2023)
[article]
Titre : Synthesis and characterization of organosilicon-modified self-matting waterborne polyurethane with excellent wear resistance Type de document : texte imprimé Auteurs : Pengfei Niu, Auteur ; Weichen Pan, Auteur ; Wei Wang, Auteur ; Meng Wang, Auteur ; Bao Zhang, Auteur ; Junfeng Yang, Auteur ; Xiaohong Peng, Auteur Année de publication : 2023 Article en page(s) : p. 1963-1976 Note générale : Bibliogr. Langues : Américain (ame) Catégories : Analyse morphologique
Caractérisation
Matériaux auto-mattants
Polymères -- Synthèse
Polymères en émulsion
Polyuréthanes
Résistance à l'usureIndex. décimale : 667.9 Revêtements et enduits Résumé : Self-matting waterborne polyurethane (WPU) with a rough surface suffers from poor wear resistance, which inevitably hinders its service span. Here, wear-resistant and self-matting WPU resin was prepared via using hydroxypropyl-terminated polydimethylsiloxane (PDMS) in the preparation of prepolymer and N-2-aminoethyl-3-aminopropyltrimethoxysilane (KH-792) as a post-chain extender. The effects of PDMS, 2, 2-Bis(hydroxymethyl)propionic acid (DMPA), and KH-792 on its morphology, particle size, gloss, wear resistance, and hydrophilicity of WPU were also investigated. The gloss of WPU coatings was found to be negatively correlated with the amount of DMPA. Moreover, the matting effect and the wear resistance of WPU were significantly enhanced by the introduction of PDMS and KH-792. When the content of PDMS, DMPA, and KH-792 was 6 wt%, 2.2 wt%, and 40 mol% respectively, the gloss was 3.2 GU, and the wear mass loss was only 6.6 mg, which was 64% lower than that without silicone-modified. This work could provide a new idea for the preparation of wear-resistant and self-matting coatings. Note de contenu : - EXPERIMENTAL : Materials - Synthesis of silicone-modified self-matting WPU - Characterization
- RESULTS AND DISCUSSION : FTIR characterization - NMR characterization - Effect of the DMPA content - Effect of the KH-792 content - SEM analysis - 3D morphology characterizationDOI : https://doi.org/10.1007/s11998-023-00790-7 En ligne : https://link.springer.com/content/pdf/10.1007/s11998-023-00790-7.pdf Format de la ressource électronique : Permalink : https://e-campus.itech.fr/pmb/opac_css/index.php?lvl=notice_display&id=40174
in JOURNAL OF COATINGS TECHNOLOGY AND RESEARCH > Vol. 20, N° 6 (11/2023) . - p. 1963-1976[article]Réservation
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Code-barres Cote Support Localisation Section Disponibilité 24337 - Périodique Bibliothèque principale Documentaires Disponible Synthesis and characterization of UV-curable cellulose acetate butyrate-based oligomers and their cotton fabric coatings / Ozan Gazi Dehmen in JOURNAL OF COATINGS TECHNOLOGY AND RESEARCH, Vol. 18, N° 4 (07/2021)
[article]
Titre : Synthesis and characterization of UV-curable cellulose acetate butyrate-based oligomers and their cotton fabric coatings Type de document : texte imprimé Auteurs : Ozan Gazi Dehmen, Auteur ; Hacen Aysen Onen, Auteur ; Zehra Yildiz, Auteur ; Atilla Güngör, Auteur ; Yalcin Boztoprak, Auteur Année de publication : 2021 Article en page(s) : p. 1075–1085 Note générale : Bibliogr. Langues : Américain (ame) Catégories : Brillance (optique)
Butyrate d'acétate de cellulose
Caractérisation
CotonLe coton est une fibre végétale qui entoure les graines des cotonniers "véritables"(Gossypium sp.), un arbuste de la famille des Malvacées. Cette fibre est généralement transformée en fil qui est tissé pour fabriquer des tissus. Le coton est la plus importante des fibres naturelles produites dans le monde. Depuis le XIXe siècle, il constitue, grâce aux progrès de l'industrialisation et de l'agronomie, la première fibre textile du monde (près de la moitié de la consommation mondiale de fibres textiles).
Enduction
Essais (technologie)
Huile de coton
Oligomères
Perméabilité
Polymères -- Synthèse
Résistance thermique
Revêtements -- Propriétés mécaniques
Revêtements organiques
Textiles et tissusIndex. décimale : 667.9 Revêtements et enduits Résumé : In order to improve the thermal stability and flexibility, cellulose acetate butyrate (CAB) was modified with toluene diisocyanate–hydroxyethyl methacrylate (TDI–HEMA) adduct in various molar ratios. The obtained oligomer was characterized by proton nuclear magnetic resonance (1H NMR) and Fourier transform infrared (FTIR) spectroscopies. Gloss, cross-hatch, contact angle, and Taber abrasion tests were all used to investigate the film forming performance of the modified CAB oligomers on glass plates. The UV-cured free films of the synthesized oligomers were examined in terms of the mechanical tests. By using the synthesized CAB oligomers, coating formulations were prepared and applied onto cotton fabrics in order to make the cotton fabrics more durable in outdoor environments. The existence of the coating layer on the fabric surfaces was investigated by scanning electron microscopy (SEM). The coated UV-cured fabrics were evaluated separately in terms of abrasion, thermal conductivity, and air and water vapor permeability properties. Results proved that the oligomer (50%-CAB) in which 50% of the hydroxyl groups of CAB were reacted with TDI–HEMA adduct showed the best mechanical properties with the highest tensile strength and modulus values. Considering the coated fabrics, the least deformation against abrasion, the highest air/water vapor permeability, and the best thermal conductivity were all recorded in 50%-CAB coated sample. Note de contenu : - EXPERIMENTAL : Materials - Synthesis of modified CAB oligomers - Coating applications on cotton fabrics - Characterization
- RESULTS AND DISCUSSION : FTIR spectra - Film forming properties on glass layers - Mechanical properties of free films
- Table 1 : Sample codes with modification percentages
- Table 2 : Gloss, cross-hatch, and contact angle test results of samples on glass plates
- Table 3 : Mechanical properties of UV-cured free films of modified CAB oligomers
- Table 4 : Abrasion test results of coated UV-cured cotton fabrics for each formulation
- Table 5 : Clothing comfort properties of coated UV-cured cotton fabrics for each formulationDOI : https://doi.org/10.1007/s11998-020-00461-5 En ligne : https://link.springer.com/content/pdf/10.1007/s11998-021-00461-5.pdf Format de la ressource électronique : Permalink : https://e-campus.itech.fr/pmb/opac_css/index.php?lvl=notice_display&id=36214
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Code-barres Cote Support Localisation Section Disponibilité 22969 - Périodique Bibliothèque principale Documentaires Disponible Synthesis and characterization of water-thinnable thermosetting acrylic resins for low-cure surface coatings / Ganesh Datt Bajpai in PAINTINDIA, Vol. LVII, N° 8 (08/2007)
[article]
Titre : Synthesis and characterization of water-thinnable thermosetting acrylic resins for low-cure surface coatings Type de document : texte imprimé Auteurs : Ganesh Datt Bajpai, Auteur ; Raju Pramod Kumar, Auteur Année de publication : 2007 Article en page(s) : p. 75-82 Note générale : Bibliogr. Langues : Anglais (eng) Catégories : Basses températures
Caractérisation
Polyacryliques
Polymères -- Synthèse
Réticulation (polymérisation)
Revêtements:Peinture
ThermodurcissablesIndex. décimale : 667.9 Revêtements et enduits Résumé : Among the various binders used for industrial finishes, thermosetting acrylics (TSAs) are gaining importance. There are two main reasons for this; firstly they possess inherently superior properties; such as water clear appearance, colour retention, good durability, low pigment reactivity, excellent chemical resistance and excellent flexibility. Secondly, thermosetting acrylics provide greater formulation latitude as they can be tailor made to suit specific applications. Presently, thermosetting acrylics are commonly used in the two major forms: (a) Solvent soluble thermosetting acrylics for conventional solids coatings. (b) Thermosetting acrylics for high solids coatings. . In the present work, water-thinnable acrylic resins have been developed wherein water is used in place of volatile organic solvent which is the main source of VOC emission. Water-thinnable thermosetting acrylics are getting more prominence day after day because of their eco-friendly nature, cost effectiveness and superior films performance. However, ordinary water-thinnable thermosetting acrylic resins cure at high temperature (≈120-150°C) and hence involve high energy consumption. Through this work, efforts have also been directed towards developing such water-thinnable thermosetting acrylic resins which can be cured at lower temperature to yield low-cure surface coatings. For achieving this, a series of TSA resins were prepared by reacting 2-hydroxy ethyl methacrylate (HEMA) and acrylic acid (AA) as monomers in butanol as solvent in presence of benzoyl peroxide as initiator. The prepared TSA resins were made water soluble by neutralizing with ammonia solution. The coating films-were then baked at 90°C for 30 minutes to effect film cure. Cured films were evaluated for their various optical, mechanical and chemical resistance properties to ascertain the commercial utility of low-temperature curable water-thinnable TSA resins. Note de contenu : Classification of TSA
- Experimental : Materials - Synthesis - Analysis - Preparation of coating films and their curing
- Results & discussion : IR-spectra - Evaluation of film properties - Mechanical propertiesPermalink : https://e-campus.itech.fr/pmb/opac_css/index.php?lvl=notice_display&id=11500
in PAINTINDIA > Vol. LVII, N° 8 (08/2007) . - p. 75-82[article]Réservation
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Code-barres Cote Support Localisation Section Disponibilité 008391 - Périodique Bibliothèque principale Documentaires Disponible Synthesis and characterization of water-thinnable thermosetting acrylic resins for low-cure surface coatings in PAINTINDIA, Vol. LVIII, N° 1 (01/2008)
[article]
Titre : Synthesis and characterization of water-thinnable thermosetting acrylic resins for low-cure surface coatings Type de document : texte imprimé Année de publication : 2008 Article en page(s) : p. 67-74 Note générale : Bibliogr. Langues : Anglais (eng) Catégories : Basses températures
Caractérisation
Copolymères
Polyacryliques
Polymères -- Synthèse
Revêtements:Peinture
ThermodurcissablesIndex. décimale : 667.9 Revêtements et enduits Résumé : Among the various binders used for industrial finishes, thermosetting acrylics (TSAs) are gaining importance. There are two main reasons for this ; firstly they possess inherently superior properties ; such as water clear appearance, colour retention, good durability, low pigment reactivity, excellent chemical resistance and excellent flexibility. Secondly, thermosetting acrylics provide greater formulation latitude as they can be tailor made to suit specific applications. Presently, thermosetting acrylics are commonly used in the two major forms: (a) Solvent soluble thermosetting acrylics for conventional solids coatings. (b) Thermosetting acrylics for high solids coatings. . In the present work, water-thinnable acrylic resins have been developed wherein water is used in place of volatile organic solvent which is the main source of VOC emission. Water-thinnable thermosetting acrylics are getting more prominence day after day because of their eco-friendly nature, cost effectiveness and superior films performance. However, ordinary water-thinnable thermosetting acrylic resins cure at high temperature (≈120-150°C) and hence involve high energy consumption. Through this work, efforts have also been directed towards developing such water-thinnable thermosetting acrylic resins which can be cured at lower temperature to yield low-cure surface coatings. For achieving this, a series of TSA resins were prepared by reacting 2-hydroxy ethyl methacrylate (HEMA) and acrylic acid (AA) as monomers in butanol as solvent in presence of benzoyl peroxide as initiator. The prepared TSA resins were made water soluble by neutralizing with ammonia solution. The coating films-were then baked at 90°C for 30 minutes to effect film cure. Cured films were evaluated for their various optical, mechanical and chemical resistance properties to ascertain the commercial utility of low-temperature curable water-thinnable TSA resins. Note de contenu : - EXPERIMENTAL : Materials - Synthesis - Analysis - Preparation of coating films and their curing
- RESULTS & DISCUSSION : IR-spectra - evaluation of film properties - Mechanical propertiesPermalink : https://e-campus.itech.fr/pmb/opac_css/index.php?lvl=notice_display&id=12091
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Code-barres Cote Support Localisation Section Disponibilité 010764 - Périodique Bibliothèque principale Documentaires Disponible Synthesis and characterization of waterborne epoxy derived from epoxidized soybean oil and bioderived C-36 dicarboxylic acid / Sukanya Pradhan in JOURNAL OF COATINGS TECHNOLOGY AND RESEARCH, Vol. 14, N° 4 (07/2017)
[article]
Titre : Synthesis and characterization of waterborne epoxy derived from epoxidized soybean oil and bioderived C-36 dicarboxylic acid Type de document : texte imprimé Auteurs : Sukanya Pradhan, Auteur ; Priyanka Pandey, Auteur ; Smita Mohanty, Auteur ; Sanjay K. Nayak, Auteur Année de publication : 2017 Article en page(s) : p. 915-926 Note générale : Bibliogr. Langues : Américain (ame) Catégories : Biomatériaux
Caractérisation
Dimère, Acide
Epoxydes
Polymères -- Synthèse
Polymères en émulsionIndex. décimale : 667.9 Revêtements et enduits Résumé : This study focuses on synthesis of waterborne epoxy (WBE) derived from epoxidized soybean oil (ESO) and its compatibility with water-dispersible curing agent Pripol 1009, which is a bioderived long-chain dimer acid. The reaction parameters involved in the synthesis of WBE from ESO have been optimized based on physicochemical properties like hydroxyl value, epoxy equivalent value and degree of solubility of WBE. The WBE obtained after 5 and 6 h of reaction time was found to be of optimum composition with balanced physicochemical properties. The mechanical, thermal and physicochemical properties of WBE obtained after 6 h of reaction time revealed relatively better performance characteristics as compared to ESO. Note de contenu : - EXPERIMENTAL : Materials and methods - Synthesis of waterborne epoxy (WBE) - Preparation of cured ESO and WBE
- CHARACTERIZATION : Solubility test - Particle size analysis - Storage stability - Solid content - Spectral analysis - Chemical resistance - Water uptake - Swelling and crosslink density determination - Mechanical analysis - Differential scanning calorimetry analysis
- RESULTS AND DISCUSSION : Physicochemical analysis of WBE - Fourier transform infrared spectroscopic (FTIR) analysis - Proton NMR analysis - Mechanical analysis - Differential scanning calorimetry (DSC) analysis - Chemicals resistance - Swelling and crosslink densigy - Water uptakeDOI : 10.1007/s11998-016-9884-3 En ligne : https://link.springer.com/content/pdf/10.1007%2Fs11998-016-9884-3.pdf Format de la ressource électronique : Permalink : https://e-campus.itech.fr/pmb/opac_css/index.php?lvl=notice_display&id=28933
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