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Preparation and characterization of melamine modified urea-formaldehyde foam / Y. Ma in INTERNATIONAL POLYMER PROCESSING, Vol. XXVIII, N° 2 (05/2013)
[article]
Titre : Preparation and characterization of melamine modified urea-formaldehyde foam Type de document : texte imprimé Auteurs : Y. Ma ; W. Zhang ; C. Wang ; Y. Xu ; S. Li ; F. Chu Année de publication : 2013 Article en page(s) : p. 188-198 Note générale : Bibliogr. Langues : Anglais (eng) Catégories : Angle de contact
Caractérisation
Combustion
Formaldéhyde
Fumée -- Analyse
Isolants
MélamineLa mélamine, de nom chimique 1,3,5-triazine-2,4,6-triamine, est parfois dénommée cyanuramide ou cyanurotriamine. Sa formule brute est C3H6N6.
Les "résines mélamine-formaldéhyde" ou "mélamine-formol" (sigle MF) sont appelées "mélamine" dans le langage courant. Elles font partie de la famille des aminoplastes qui regroupe des résines thermodurcissables aminées, issues d'un comonomère tel l'urée ou la mélamine, parfois le thiocarbamide, le cyanamide hydrogène ou le dicyandiamide ; le second comonomère étant le formaldéhyde.
Mousses plastiques
Mousses plastiques -- Propriétés mécaniques
Polymères
Résistance à l'humidité
Résistance à la compression
Réticulants
Surfactants
Thermocinétique
UréeIndex. décimale : 668.9 Polymères Résumé : Melamine-urea-formaldehyde (MUF) foam was prepared using melamine modified urea formaldehyde resin. The effects of blowing agent, curing agent and surfactant on the properties of MUF foam such as apparent densities, compression strength, microstructure, fragility, limited oxygen index, thermal conductivity and formaldehyde emission were investigated. The best performance of MUF was obtained as the composition of blowing agent, curing agent and surfactant were 2.5 %, 18 % and 12 % respectively. The water resistance of MUF foam, contents of foam’s burning gas, curing mechanism and physical properties were also studied by Contact angle analyzer, TGA-FT-IR, FT-IR and 13C NMR. Note de contenu : - EXPERIMENTAL : Materials - MUF resin and foam preparation - Characterizations of MUF foam - SEM analysis of MUF foam - Contact angle measurements - TGA-FT-IR analysis of MUF foam - FT-IR analysis of MUF resin and foam - Liquid C NMR analysis of MUF resin - Solid C NMR analysis of MUF foam
- RESULTS AND DISCUSSION : The influence of the blowing agent amount on the MUF foam properties - The influence surfactant amount on MUF foam properties - The influence curing agent amount on MUF foam properties - Water resistance of MUF foam - TGA-FT-IR analysis of MUF foam - FT-IR analysis of MUF resin and foam - C NMR spectrogram of MUF resin and foamDOI : 10.3139/217.2684 En ligne : https://drive.google.com/file/d/1CEUpiEWVqVziV5KzXAN1uOSCCzIUYd28/view?usp=drive [...] Format de la ressource électronique : Permalink : https://e-campus.itech.fr/pmb/opac_css/index.php?lvl=notice_display&id=18432
in INTERNATIONAL POLYMER PROCESSING > Vol. XXVIII, N° 2 (05/2013) . - p. 188-198[article]Réservation
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Code-barres Cote Support Localisation Section Disponibilité 15050 - Périodique Bibliothèque principale Documentaires Disponible Preparation and characterization of modified protein retanning agent based on leather waste / Wang Xuechuan in JOURNAL OF THE SOCIETY OF LEATHER TECHNOLOGISTS & CHEMISTS (JSLTC), Vol. 100, N° 3 (05-06/2016)
[article]
Titre : Preparation and characterization of modified protein retanning agent based on leather waste Type de document : texte imprimé Auteurs : Wang Xuechuan, Auteur ; Zhang Ting, Auteur ; Ren Longfang, Auteur ; Qiang Taotao, Auteur Année de publication : 2016 Article en page(s) : p. 136-141 Note générale : Bibliogr. Langues : Anglais (eng) Catégories : Acrylate de butyle
Agents de tannage
Caractérisation
Collagène
Cuirs et peaux -- Déchets -- Recyclage
Cuirs et peaux -- Propriétés mécaniques
Cuirs et peaux de chèvres
Greffage (chimie)
Retannage
StyrèneIndex. décimale : 675.2 Préparation du cuir naturel. Tannage Résumé : Collagen extracted from leather wastes was used as the main raw material, a modified protein retanning agent was prepared by free radical polymerization reaction with butyl acrylate and styrene. The product was characterized by FT-IR, TEM, particle size analysis and other methods. The retanning properties were studied on goat garment leather. The results showed that grafting took place between collagen and the non-ionic monomers. The grafting rate was about 65%. The latex particles of the modified collagen cross-linking emulsion were spherical and uniform, the average particle size was about 117nm. The resistances of the product to electrolyte, acid and alkali were good. The thickening rate [substance increase] of the leather was about 10% when using the retanning agent. The leather has good resistance to wet and dry rubbing after retanning, the fixing effect was remarkable. The shrinkage temperature was up to 122°C. Compared with similar commercial retanning agents, the tensile strength and tearing strength of leather retanned by the self-prepared retanning agent increased by 28.5% and 37.8%, respectively. Note de contenu : - EXPERIMENTAL PROCEDURES : Reagents and apparatus - Preparation of modified collagen retanning agent - Characterization - The application of collagen retanning agent on leather
- RESULTS AND DISCUSSION : Characterization of modified collagen retanning agent - The application of collagen retanning agent in leatherEn ligne : https://drive.google.com/file/d/1flVupBNcHccMn5FrnO29d9kywrKG8Yky/view?usp=drive [...] Format de la ressource électronique : Permalink : https://e-campus.itech.fr/pmb/opac_css/index.php?lvl=notice_display&id=26447
in JOURNAL OF THE SOCIETY OF LEATHER TECHNOLOGISTS & CHEMISTS (JSLTC) > Vol. 100, N° 3 (05-06/2016) . - p. 136-141[article]Réservation
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Code-barres Cote Support Localisation Section Disponibilité 18140 - Périodique Bibliothèque principale Documentaires Disponible Preparation and characterization of nano-reinforced leather waste fiber-epoxy nano composite / Venkatasubramanian Sivakumar in JOURNAL OF THE AMERICAN LEATHER CHEMISTS ASSOCIATION (JALCA), Vol. CX, N° 12 (12/2015)
[article]
Titre : Preparation and characterization of nano-reinforced leather waste fiber-epoxy nano composite Type de document : texte imprimé Auteurs : Venkatasubramanian Sivakumar, Auteur ; T. R. Swathi, Auteur ; Resmi Mohan, Auteur ; Asit Baran Mandal, Auteur Année de publication : 2015 Article en page(s) : p. 401-408 Note générale : Bibliogr. Langues : Américain (ame) Catégories : Caractérisation
Composites à fibres
Cuirs et peaux -- Déchets -- Recyclage
Dioxyde de titane
Epoxydes
Fibres animales
Nanoparticules
Résistance chimique
solvants
Stabilité thermiqueIndex. décimale : 675 Technologie du cuir et de la fourrure Résumé : Significant quantities of leather waste fibers are generated from the leather industry. Confinement and utilization of leather waste fibers by converting them in to useful materials such as nano-composites is desirable. Earlier studies on making composites from leather waste fibers suffer from strength properties for different applications. In this paper, preparation and characterization of nano composite from leather fiber–epoxy polymer reinforced with nano TiO2 has been studied and reported for the first time. Physical testing of these nano composites shows better strength and other properties for improved performance as versatile material. TGA and DSC studies revealed better thermal stability (up to 330°C) for these nano composites. FTIR analysis shows possible chemical interaction between epoxy polymer and leather fiber. Better solvent resistant property was also noticed for the nano-composites prepared. SEM analysis indicates uniform nano-composite structure and distribution of nano TiO2 in the matrix. The present approach not only offers a solution to the disposal problem regarding leather solid wastes like buffing dusts, but also offers a versatile nano composite material. Note de contenu : - INTRODUCTION : Nano-composites using leather waste fibers - Literature survey on composites from leather wastes - Drawbacks of earlier processes/products - Objectives of the present work
- EXPERIMENTAL : Materials - Preparation of nano-composite from buffing dust - Testing of nano-composites from buffing dust - Scanning electron microscopic (SEM) analysis
- RESULTS AND DISCUSSIONS : Nano-composite utilizing leather waste fiber and epoxy - Hardness test - Tensile strength - Thermogravimetric analysis (TGA) - Differential scanning calorimetry (DSC) - Fourier Transform Infrared Spectroscopy (FT-IR) - Chemical resistance test - Scanning electron microscopic (SEM) analysisEn ligne : https://drive.google.com/file/d/1GY7pvH70zUbI01gMsveF5Zny_FPRn_BJ/view?usp=drive [...] Format de la ressource électronique : Permalink : https://e-campus.itech.fr/pmb/opac_css/index.php?lvl=notice_display&id=25050
in JOURNAL OF THE AMERICAN LEATHER CHEMISTS ASSOCIATION (JALCA) > Vol. CX, N° 12 (12/2015) . - p. 401-408[article]Réservation
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Code-barres Cote Support Localisation Section Disponibilité 17652 - Périodique Bibliothèque principale Documentaires Disponible Preparation and characterization of nanocrystalline and mesoporous strontium titanate thin films at room temperature / M. Mohammadi in JOURNAL OF COATINGS TECHNOLOGY AND RESEARCH, Vol. 8, N° 5 (10/2011)
[article]
Titre : Preparation and characterization of nanocrystalline and mesoporous strontium titanate thin films at room temperature Type de document : texte imprimé Auteurs : M. Mohammadi, Auteur ; D. J. Fray, Auteur Année de publication : 2011 Article en page(s) : p. 585-593 Note générale : Bibliogr. Langues : Américain (ame) Catégories : Caractérisation
Matériaux nanocristallins
Sol-gel, Procédé
Température de laboratoire
Titanate de strontiumIndex. décimale : 667.9 Revêtements et enduits Résumé : The low temperature perovskite-type strontium titanate (SrTiO3) thin films and powders with nanocrystalline and mesoporous structure were prepared by a straightforward particulate sol–gel route. The prepared sol had a narrow particle size distribution with hydrodynamic diameter of about 17 nm. X-ray diffraction (XRD) revealed that the synthesized powders had a perovskite-SrTiO3 structure with preferable orientation growth along the (1 0 0) direction. TEM images showed that the average crystallite size of the powders annealed in the range 300–800°C was around 8 nm. FE-SEM analysis and AFM images revealed that the deposited thin films had mesoporous and nanocrystalline structure with the average grain size of 25 nm at 600°C. Based on Brunauer–Emmett–Taylor (BET) analysis, the synthesized powders showed mesoporous structure with BET surface area in the range 92–75 m2/g at 400–600°C. One of the smallest crystallite sizes and one of the highest surface areas reported in the literature were obtained, which can be used in many applications, such as photocatalysts. Note de contenu : EXPERIMENTAL : Preparation of the strontium titanate sol - Preparation of strontium titanate thin films - Synthesis of strontium titanate powders.
RESULTS AND DISCUSSION : Particle size - Crystal characterization - Thermal analysis - Microstructure - Specific surface area.DOI : 10.1007/s11998-011-9347-9 En ligne : https://link.springer.com/content/pdf/10.1007%2Fs11998-011-9347-9.pdf Format de la ressource électronique : Permalink : https://e-campus.itech.fr/pmb/opac_css/index.php?lvl=notice_display&id=12234
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Code-barres Cote Support Localisation Section Disponibilité 13360 - Périodique Bibliothèque principale Documentaires Disponible Preparation and characterization of new antifouling coating based on alkyd paint modified with hydrophobic cationic biocide in JOURNAL OF COATINGS TECHNOLOGY AND RESEARCH, Vol. 21, N° 3 (05/2024)
[article]
Titre : Preparation and characterization of new antifouling coating based on alkyd paint modified with hydrophobic cationic biocide Type de document : texte imprimé Année de publication : 2024 Article en page(s) : p. 939-953 Note générale : Bibliogr. Langues : Américain (ame) Catégories : Antimicrobiens
Biofilms
Caractérisation
Hydrophobie
Polyalkydes
Revêtements antisalissures:Peinture antisalissures
Revêtements organiquesIndex. décimale : 667.9 Revêtements et enduits Résumé : New water-immiscible cationic biocide 1-dodecylpyridinium dodecylbenzenesulfonate (PyrC12-DBS) has been synthesized and tested as potential antifouling agent for commercial alkyd paint PP-115 (Ukraine). The modified PP-115/PyrC12-DBS coatings containing 8% and 16% (w/w) of PyrC12-DBS were prepared by dissolution directly of the cationic biocide into the PP-115 paint. Once the stainless steel bars were painted, the surface wettability of the coating was found to be significantly increased when modified with cationic biocide. The results of scanning electron microscopy (SEM) and energy-dispersive X-ray spectroscopy (EDX) studies indicate high homogeneity of the modified coatings. Infrared analysis revealed hydrogen bonding between ester groups of alkyd resin and pyridinium cations of PyrC12-DBS. The plasticizing effect of the cationic biocide on the alkyd binder has also been revealed by differential scanning calorimetry analysis. According to spectrophotometric analysis data, PyrC12-DBS has excellent resistance to leaching from protective coatings into water. Antibiofilm efficiency of PyrC12-DBS was evaluated by assessing the capability of two biofilm-forming model strains, namely Staphylococcus aureus ATCC 25923 and Pseudomonas aeruginosa PA01, to form attached biofilms on the surface coated with modified alkyd paint. A significant decrease in biofilm metabolic activity, as well as in cell biomass, was determined for PP-115/PyrC12-DBS (16%) coatings. The antifouling activity was evaluated by exposure to experimental substrates in freshwater (Dnipro River) for 143 days. The surface of PP-115/PyrC12-DBS (16%) coatings showed an almost 13-fold reduction of total biomass formed by Dreissenidae mussels compared with control substrates. Overall, the obtained data indicate that the contact-active protective coatings based on water-insoluble polymer matrix and water-insoluble cationic biocide may effectively resist biofouling at relatively high biocide content. Note de contenu : - MATERIALS AND METHODS : Materials - Preparation of antifouling coating - Characterization of prepared coatings
- RSULTS AND DISCUSSION : IR analysis - Morphological and surface properties - Raman imaging - EDX imaging - DSC analysis 6 Leaching resistance of PyrC12-DBSDOI : https://doi.org/10.1007/s11998-023-00862-8 En ligne : https://link.springer.com/content/pdf/10.1007/s11998-023-00862-8.pdf Format de la ressource électronique : Permalink : https://e-campus.itech.fr/pmb/opac_css/index.php?lvl=notice_display&id=41068
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