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Optical and temperature dependent electrical properties of poly (vinyl chloride)/copper alumina nanocomposites for optoelectronic devices / S. Suvarna in INTERNATIONAL POLYMER PROCESSING, Vol. 38, N° 2 (2023)
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Titre : Optical and temperature dependent electrical properties of poly (vinyl chloride)/copper alumina nanocomposites for optoelectronic devices Type de document : texte imprimé Auteurs : S. Suvarna, Auteur ; Annumaria Sebastian, Auteur ; Furhan, Auteur ; Manammel Thankappan Ramesan, Auteur Année de publication : 2023 Article en page(s) : p. 154-156 Note générale : Bibliogr. Langues : Anglais (eng) Catégories : Alumine
Caractérisation
Chlorure de polyvinyle
Composites -- Propriétés optiques
Cuivre
Diélectriques
Matériaux hybrides
Modèles mathématiques
Stabilité thermique
ThermocinétiqueIndex. décimale : 668.4 Plastiques, vinyles Résumé : The practical applications of poly (vinyl chloride) have been constrained due to its poor thermal stability, low dielectric constant and inability to shield against ultraviolet (UV) radiation. In this study, we tried to improve the optical properties, thermal stability, temperature-dependent electrical conductivity and dielectric constant using copper alumina (Cu–Al2O3) nanoparticles reinforced poly (vinyl chloride) (PVC). Optical absorption measured with an ultraviolet-visible (UV-visible) spectrometer emphasises the blueshift in absorption edges and decreasing bandgap energies of PVC/Cu–Al2O3 nanocomposites compared to PVC. The presence of Cu–Al2O3 in PVC and its interaction with the polymer were confirmed by FTIR spectroscopy. Thermogravimetric analysis (TGA) demonstrates that nanocomposites have higher thermal stability than PVC, and that thermal stability increases with filler loading. Scanning electron microscopy (SEM) indicates the homogeneous dispersion of nanosized Cu–Al2O3 in the polymer matrix. The activation energy determined by the Arrhenius equation revealed that AC conductivity increases with the addition of nanoparticles up to a specific loading. The dielectric constant increases as a function of temperature and decreases with frequency. The magnitude of AC conductivity and dielectric constant were highest for 7 wt% loaded nanocomposites. The dielectric constant predicted by the Bruggeman and Maxwell-Garnet models were in good agreement with the experimental permittivity. The semiconducting nature of nanocomposites was investigated by impedance analysis. The semi-circular nature of Cole-Cole plots manifests the combination of parallel capacitance with low bulk resistance. The enhanced optical, thermal, electrical and dielectric properties of PVC/Cu–Al2O3 nanocomposites can be utilized in fabricating optoelectronic devices with excellent charge-storing ability. Note de contenu : - EXPERIMENTAL : Materials and methods - Synthesis of copper alumina nanoparticles - Preparation of poly (vinyl chloride)/copper alumina nanocomposites - Characterizations
- RESULTS AND DISCUSSION : UV-visible spectroscopy - Optical bandgap energy - Fourier transform IR spectroscopy - SEM analysis - Thermogravimetric analysis - AC conductivity - Dielectric constant - Dielectric modelling - Impedance studies
- Table 1 : Activation energy of PVC/Cu–Al2O3 nanocomposites at different frequenciesDOI : https://doi.org/10.1515/ipp-2022-4270 En ligne : https://drive.google.com/file/d/1PiSW7w4CgwZjlcALwPviqWqCkaTm2GKW/view?usp=drive [...] Format de la ressource électronique : Permalink : https://e-campus.itech.fr/pmb/opac_css/index.php?lvl=notice_display&id=39498
in INTERNATIONAL POLYMER PROCESSING > Vol. 38, N° 2 (2023) . - p. 154-156[article]Réservation
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Code-barres Cote Support Localisation Section Disponibilité 24121 - Périodique Bibliothèque principale Documentaires Disponible Optimisation of ultrasonic-assisted extraction of natural dyes from pomegranate rind using response surface methodology and its characterisation / TengFei Lei in COLORATION TECHNOLOGY, Vol. 137, N° 3 (06/2021)
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Titre : Optimisation of ultrasonic-assisted extraction of natural dyes from pomegranate rind using response surface methodology and its characterisation Type de document : texte imprimé Auteurs : TengFei Lei, Auteur ; Ying Pan, Auteur ; Bin Zhang, Auteur ; RongZhan Liu, Auteur ; YuanFeng Pan, Auteur Année de publication : 2021 Article en page(s) : p. 259-271 Note générale : Bibliogr. Langues : Anglais (eng) Catégories : Antibactériens
Antioxydants
Caractérisation
Colorants végétaux
Extraction par ultrasons
Fourier, Spectroscopie infrarouge à transformée de
Grenade (fruit) et constituants
Mesure
Plan d'expérience
Teinture -- Fibres textilesIndex. décimale : 667.2 Colorants et pigments Résumé : This paper reports the optimal ultrasonic-assisted extraction (UAE) conditions for the maximum recovery of natural dyes from pomegranate rind using response surface methodology. The optimum UAE conditions were found to be an extraction time of 60 minutes, an extraction temperature of 65°C, a water to material ratio of 19 mL/g and an ultrasonic power of 132 W. The yield of the extracted pomegranate rind dyes (PRD) under optimum conditions was 17.1% ± 0.1%, which closely agrees with the predicted value of 17.2%. Fourier Transform–infrared and ultraviolet-visible absorption spectroscopy indicated that there were no significant structural changes in the PRD under optimal UAE conditions. The PRD particle size was clearly reduced, and the distribution was more uniform under the action of the ultrasonic waves. The total anti-oxidant activity of the PRD was analysed using DPPH• assay, and the results indicated that a proper and reasonable ultrasonic-assisted treatment can enhance the anti-oxidant capacity of the pomegranate rind natural dyes. Furthermore, in comparison with Staphylococcus aureus using the Agar plate method, the anti-bacterial activity indicated that the fabrics dyed with PRD under UAE conditions displayed outstanding anti-bacterial activity. Note de contenu : - EXPERIMENTAL : Materials - PRD extraction procedure - Measurements - Experimental design
- RESULTS AND DISCUSSION : Optimisation of the UAE conditions by RSMDOI : https://doi.org/10.1111/cote.12528 En ligne : https://onlinelibrary.wiley.com/doi/epdf/10.1111/cote.12528 Format de la ressource électronique : Permalink : https://e-campus.itech.fr/pmb/opac_css/index.php?lvl=notice_display&id=36092
in COLORATION TECHNOLOGY > Vol. 137, N° 3 (06/2021) . - p. 259-271[article]Réservation
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Code-barres Cote Support Localisation Section Disponibilité 22845 - Périodique Bibliothèque principale Documentaires Disponible Optimising conditions for preparing collagen-type hydrolysates / Pavel Mokrejs in JOURNAL OF THE SOCIETY OF LEATHER TECHNOLOGISTS & CHEMISTS (JSLTC), Vol. 100, N° 3 (05-06/2016)
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Titre : Optimising conditions for preparing collagen-type hydrolysates Type de document : texte imprimé Auteurs : Pavel Mokrejs, Auteur ; Dagmar Janacova, Auteur ; Lubomir Benicek, Auteur ; Tomas Plachy, Auteur ; Petr Svoboda, Auteur Année de publication : 2016 Article en page(s) : p. 114-121 Note générale : Bibliogr. Langues : Anglais (eng) Catégories : Caractérisation
Collagène
Déchets organiques -- Recyclage
Hydrolysats de protéines
Hydrolyse enzymatique
Tendons -- RecyclageIndex. décimale : 675 Technologie du cuir et de la fourrure Résumé : Tendons of slaughterhouse cattle are by-products in animal processing and contain a substantial proportion of collagen and also elastin. This contribution deals with preparing collagen-type hydrolysates from cattle tendons (long tendons, hind tendons, Achilles tendons, fore tendons) in a 3-stage process. Factors under investigation are effects of added enzyme and extraction temperature on efficiency of hydrolysis. The character of starting raw materials and technological conditions in hydrolysate preparation markedly affect hydrolysis efficiency. Lower efficiency of hydrolysis (percentage of starting material converted into hydrolysate), max. 30%, is achieved when processing long tendons containing a higher elastin proportion. On the contrary, when processing hind, Achilles and fore tendons, conversion nears 100%, thus evaluating starting raw material to the utmost. Hydrolysates prepared under defined conditions (adequate addition of enzyme and suitably chosen extraction temperature) from these tendons meet strict standards specifying ash content (2.0%) for food or pharmaceutical applications. High efficiency and variability of technological conditions in the processing of cattle tendons enables to prepare high quality products (hydrolysates or gelatines) suitable for food, cosmetics or pharmaceutical applications. Note de contenu : - TABLES : 1. Composition of cattle tendons - 2. Results of hydrolysis efficiency in cattle tendons processing - 3. Composition of collagen hydrolysates prepared from cattle tendons
- FIGURES : 1. Flow chart of preparing collagen-based hydrolysates - 2. Influence of temperature and enzyme quantity on hydrolysis efficiency - 3. Influence of temperature and enzyme quantity on ash content hydrolysatesEn ligne : https://drive.google.com/file/d/1VXbOnTyDqH9_4HDew2CbmzE_yJbcC9A7/view?usp=drive [...] Format de la ressource électronique : Permalink : https://e-campus.itech.fr/pmb/opac_css/index.php?lvl=notice_display&id=26443
in JOURNAL OF THE SOCIETY OF LEATHER TECHNOLOGISTS & CHEMISTS (JSLTC) > Vol. 100, N° 3 (05-06/2016) . - p. 114-121[article]Réservation
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Code-barres Cote Support Localisation Section Disponibilité 18140 - Périodique Bibliothèque principale Documentaires Disponible Optimization and application of chromium-resistant collagenase production by Serratia sp. G / Bijun Zheng in JOURNAL OF THE SOCIETY OF LEATHER TECHNOLOGISTS & CHEMISTS (JSLTC), Vol. 108, N° 2 (03-04/2024)
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Titre : Optimization and application of chromium-resistant collagenase production by Serratia sp. G Type de document : texte imprimé Auteurs : Bijun Zheng, Auteur ; Yi Yang, Auteur ; Guangyang Jiang, Auteur ; Shihao Zhang, Auteur ; Xiaoguang Li, Auteur ; Jianfei Zhou, Auteur ; Yongqiang Tian, Auteur Année de publication : 2024 Article en page(s) : p. 78-85 Note générale : Bibliogr. Langues : Anglais (eng) Catégories : Analyse de variance En statistique, l'analyse de la variance (terme souvent abrégé par le terme anglais ANOVA : ANalysis Of VAriance) est un ensemble de modèles statistiques utilisés pour vérifier si les moyennes des groupes proviennent d'une même population. Les groupes correspondent aux modalités d'une variable qualitative (p. ex. variable : traitement; modalités : programme d'entrainement sportif, suppléments alimentaires ; placebo) et les moyennes sont calculés à partir d'une variable continue (p. ex. gain musculaire).
Ce test s'applique lorsque l'on mesure une ou plusieurs variables explicatives catégorielles (appelées alors facteurs de variabilité, leurs différentes modalités étant parfois appelées "niveaux") qui ont de l'influence sur la loi d'une variable continue à expliquer. On parle d'analyse à un facteur lorsque l'analyse porte sur un modèle décrit par un seul facteur de variabilité, d'analyse à deux facteurs ou d'analyse multifactorielle sinon. (Wikipedia)
Caractérisation
CollagénasesLes collagénases sont des enzymes capables de rompre les liaisons peptidiques du collagène. Elles facilitent la destruction des structures extracellulaires lors de la pathogenèse bactérienne. Ce sont des exotoxines.
La production de collagénases peut être induite lors d'une réponse immunitaire, par les cytokines qui stimulent les cellules telles que les fibroblastes et les ostéoplastes et occasionnent indirectement des lésions tissulaires.
Cuirs et peaux -- Détérioration
Détérioration enzymatique
Production
Serratia marcescensSerratia marcescens est une espèce de bactérie, de bacille à Gram négatif de la famille des Yersiniaceae. Un agent pathogène humain, S. marcescens est impliqué dans des infections nosocomiales, en particulier des bactériémies dans des voies veineuses centrales, des infections urinaires et des infections de plaies. On le trouve couramment dans les voies respiratoires et urinaires d'adultes hospitalisés et dans le système gastro-intestinal des enfants. En raison de sa présence abondante dans l’environnement et de sa préférence pour la vapeur, S. marcescens se trouve généralement dans les salles de bains (notamment sur les jointures de carrelage, les coins de douche, les conduites d'eau de toilette et les lavabos), où il se manifeste par une coloration orangée ou orange et une pellicule visqueuse se nourrissant de matières contenant du phosphore ou des corps gras.
Une fois établi, l'éradication complète de l'organisme est souvent difficile, mais peut être réalisée en appliquant un désinfectant à base d'eau de Javel. Le rinçage et séchage des surfaces peut prévenir son développement.
S. marcescens peut également être trouvé dans des environnements tels que la saleté, des sites supposément « stériles » et le biofilm sous-gingival des dents. Pour cette raison, et parce que S. marcescens produit un pigment de tripyrrole rouge orangé appelé prodigiosine, il peut provoquer une coloration des dents. La voie biochimique pour la production de prodigiosine par S. marcescens est inconnue à l'exception des deux dernières étapes. Dans ces étapes, un monopyrrole et un bipyrrole subissent une réaction de condensation au moyen d'une enzyme pour former de la prodigiosine. (Wikipedia)
Tannage au chromeIndex. décimale : 675.2 Préparation du cuir naturel. Tannage Résumé : This study presents a valuable chromium-resistant collagenase-producing strain (Serratia sp. G) isolated from chrome tanned leather shavings (CTLS). Optimization of its enzyme activity and subsequent practical application are thoroughly addressed. Following isolation, comprehensive optimization of the fermentation medium and culture conditions was conducted, with the most suitable components (g/L) being as follows: Maltose (15), Tryptone (25), NaH2PO4·2H2O (0.5), CaCl2 (0.05), K2HPO4·3H2O (2.5). The maximum collagenase production was attained under the conditions of a 5% inoculum, 100 mL filling volume, and incubation at 37°C with a pH of 8.5 for a duration of 48 hours. Cu2+ completely inhibited the activity of crude enzyme while Zn2+ and Mg2+ exhibited an enhancing effect on the activity of the it. Subjecting chromium-tanned leather to crude chromium-resistant collagenase at 37°C for 48 hours revealed noticeable structural alterations. Specifically, the enzymes caused visible erosion, leading to the destruction of the leather structure and the occurrence of tearing on the leather surface. Note de contenu : - MATERIALS AND METHODS : Screening of collagenase-producing strains - Determination of enzyme activity - Chromium tolerance of bacterial strains and collagenases - Optimization of fermentation conditions - Characterization of enzymatic properties - Collagenase degradation of Chromium-tanned leather
- RESULTS : Identification of collagenase-producing bacteria - Analysis of chromium tolerance in Serratia marcescens and collagenase - Optimization of fermentation conditions and RSM - Effect of temperature on enzyme activity and stability - Effect of pH on enzyme activity and stability - Effect of metal ions on enzyme activity - Analysis of collagenase degradation of chromium-tanned leather
- Table 1 : Factors and levels for RSM
- Table 2 : ANOVA for Quadratic modelEn ligne : https://drive.google.com/file/d/1iHnIVctMVNcwKCAOQ6SdYT8-e5mB_Ssi/view?usp=drive [...] Format de la ressource électronique : Permalink : https://e-campus.itech.fr/pmb/opac_css/index.php?lvl=notice_display&id=40934
in JOURNAL OF THE SOCIETY OF LEATHER TECHNOLOGISTS & CHEMISTS (JSLTC) > Vol. 108, N° 2 (03-04/2024) . - p. 78-85[article]Optimization and application of a low-density epoxy composite coating for autonomous air-to-deep sea vehicles / Michael J. Grzenda in JOURNAL OF COATINGS TECHNOLOGY AND RESEARCH, Vol. 19, N° 5 (09/2022)
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Titre : Optimization and application of a low-density epoxy composite coating for autonomous air-to-deep sea vehicles Type de document : texte imprimé Auteurs : Michael J. Grzenda, Auteur ; Marco M. Maia, Auteur ; Aristedes Costeas, Auteur ; Paul N. Ferri, Auteur ; Francisco Javier Diez, Auteur ; Jonathan P. Singer, Auteur Année de publication : 2022 Article en page(s) : p. 1523-1534 Note générale : Bibliogr. Langues : Américain (ame) Catégories : Caractérisation
Electronique -- Matériaux
Epoxydes
Matériaux hybrides
Revêtements organiques
Revêtements protecteurs
Sous-marins
ThermocinétiqueIndex. décimale : 667.9 Revêtements et enduits Résumé : Unmanned, autonomous air-to-sea vehicles, fully capable of transitioning between the two mediums, have only recently become technologically possible and have attracted great interest due to their numerous applications. However, current vehicles are unable to withstand the environmental conditions of the deep sea, especially with regards to their electronics. Previous methods for protecting electronics in the deep sea are not optimized for transitions to air. Here, a novel, lightweight, thermally-conductive, easily processed, mechanically robust, epoxy-based nanocomposite coating is presented. This material was developed with the intention of bringing the multi-domain air-water drone, known as the Naviator, to the deep ocean. In this work, the coating is thoroughly characterized and demonstrated to protect electronics submerged in water at high-pressure benchtop conditions as well as in an actual deep sea mission. The coating is also contrasted against unmodified epoxy, as well as commercial syntactic foam, and deemed superior for this application. Note de contenu : - EXPERIMENTAL SECTION : Methodology - Materials - Processing - Characterization - Benchtop testing
- RESULTS AND DISCUSSION : Material characterization - Material performance
- Table 1 : Notable aerial-aquatic vehicles
- Table 2 : All tests performed on the same nanocomposite ESC board in orderDOI : https://doi.org/10.1007/s11998-022-00627-9 En ligne : https://link.springer.com/content/pdf/10.1007/s11998-022-00627-9.pdf Format de la ressource électronique : Permalink : https://e-campus.itech.fr/pmb/opac_css/index.php?lvl=notice_display&id=38287
in JOURNAL OF COATINGS TECHNOLOGY AND RESEARCH > Vol. 19, N° 5 (09/2022) . - p. 1523-1534[article]Réservation
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