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Multiscale physical characterization of an outdoor-exposed polymeric coating system / Xiaohong Gu in JOURNAL OF COATINGS TECHNOLOGY AND RESEARCH, Vol. 6, N° 1 (03/2009)
[article]
Titre : Multiscale physical characterization of an outdoor-exposed polymeric coating system Type de document : texte imprimé Auteurs : Xiaohong Gu, Auteur ; Li-Piin Sung, Auteur ; Bouchra Kidah, Auteur ; Mounina Oudina, Auteur ; Cyril Clerici, Auteur ; Hu Haiqing, Auteur ; Debbie Stanley, Auteur ; Walter E. Byrd, Auteur ; Jerry Y. C. Jean, Auteur ; Tinh Nguyen, Auteur ; Jonathan W. Martin, Auteur Année de publication : 2009 Article en page(s) : p. 67-79 Note générale : Bibliogr. Langues : Américain (ame) Catégories : Analyse multiéchelle
Brillance (optique)
Caractérisation
Dispersion rotatoire (optique)
Microscopie à force atomique
Microscopie confocale
Morphologie (matériaux)
Optique
Revêtements protecteurs
RugositéIndex. décimale : 667.9 Revêtements et enduits Résumé : Surface topography and gloss are two related properties affecting the appearance of a polymeric coating system. Upon exposure to ultraviolet (UV) radiation, the surface topography of a coating becomes more pronounced and, correspondingly, its gloss generally decreases. However, the surface factors affecting gloss and appearance are difficult to ascertain. In this article, atomic force microscopy (AFM) and laser scanning confocal microscopy (LSCM) measurements have been performed on an amine-cured epoxy coating system exposed to outdoor environments in Gaithersburg, Maryland. The formation of the protuberances is observed at the early degradation stages, followed by the appearance of circular pits as exposure continues. At long exposure times, the circular features enlarge and deepen, resulting in a rough surface topography and crack formation. Fourier Transform Infrared Spectroscopy (FTIR) study indicates that the oxidation and chain scission reactions are likely the origins of the surface morphological changes. The relationship between changes in surface roughness and gloss has been analyzed. The root mean square (RMS) roughness of the coating is related to nanoscale and microscale morphological changes in the surface of the coating as well as to the gloss retention. A near-linear dependence of RMS roughness with the measurement length scale (L) is found on a double logarithmic scale, i.e., RMS ~ L f. The scaling factor, f, decreases with exposure time. The relationship between surface topography, on nano- to microscales, and the macroscale optical properties such as gloss retention is discussed. Moreover, a recent development in using an angle-resolved light scattering technique for the measurement of the specular and off-specular reflectance of the UV-exposed specimens is also demonstrated, and the optical scattering data are compared to the gloss and the roughness results. DOI : 10.1007/s11998-008-9108-6 En ligne : https://link.springer.com/content/pdf/10.1007%2Fs11998-008-9108-6.pdf Format de la ressource électronique : Permalink : https://e-campus.itech.fr/pmb/opac_css/index.php?lvl=notice_display&id=4860
in JOURNAL OF COATINGS TECHNOLOGY AND RESEARCH > Vol. 6, N° 1 (03/2009) . - p. 67-79[article]Réservation
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Code-barres Cote Support Localisation Section Disponibilité 011246 - Périodique Bibliothèque principale Documentaires Disponible 011271 - Périodique Bibliothèque principale Documentaires Disponible Nanoclay migration and the rheological response of PBAT-LDPE blends / M. Nofar in INTERNATIONAL POLYMER PROCESSING, Vol. 36, N° 3 (2021)
[article]
Titre : Nanoclay migration and the rheological response of PBAT-LDPE blends Type de document : texte imprimé Auteurs : M. Nofar, Auteur ; M. Mohammadi, Auteur ; P. J. Carreau, Auteur Année de publication : 2021 Article en page(s) : p. 287-296 Note générale : Bibliogr. Langues : Anglais (eng) Catégories : Alliages polymères
Argile
Cloisite
Energie de surface
Morphologie (matériaux)
Nanoparticules
Polybutylène-adipate-téréphtalate
Polyéthylène basse densité
Rhéologie
Tension superficielleIndex. décimale : 668.4 Plastiques, vinyles Résumé : Blends of a poly(butylene adipate-co-terephthalate) (PBAT) and a low density polyethylene (LDPE) (80 wt%/20 wt%) were prepared through a twin screw extruder while incorporating 3 wt% Cloisite 30B (C30B) nanoclay that possessed a much higher affinity with PBAT. The blends were processed through three melt mixing strategies: ( i) direct mixing of all three components, (ii) mixing C30B and PBAT followed by mixing with LDPE, and (iii) mixing C30B and LDPE followed by mixing with PBAT. The rheological properties of each system were determined in small amplitude oscillatory shear (SAOS) experiments. The migration of C30B nanoparticles from the LDPE minor phase towards the PBAT matrix was then monitored in the blend nanocomposites prepared through strategy (iii) via SAOS time sweep experiments. It was firstly understood that the C30B migration could be detected during time sweep SAOS experiments. The migration time was observed to be frequency dependent due to the smaller length scales probed at larger frequencies. Such migration occurred even faster when the SAOS time sweep experiments were conducted at a higher temperature due to the viscosity reduction. Note de contenu : - EXPERIMENTAL : Materials - Melt compounding and blend nanocomposite preparation - Surface energy, interfacial tension, and localization analysis - Morphological analysis - Rheological measurements
- RESULTS AND DISCUSSION : Characteristics of neat polymers and c30b localization - Morphological and rheological properties of the blend and blend nanocomposites - Monitoring C30B migration through SAOS experiments - Relationship between nanoparticle migration, applied frequency, and LDPE viscosityDOI : https://doi.org/10.1515/ipp-2020-4057 En ligne : https://drive.google.com/file/d/1XhPD0BX6SWTIUyaH0mkZ-xOdYeN3qEoS/view?usp=shari [...] Format de la ressource électronique : Permalink : https://e-campus.itech.fr/pmb/opac_css/index.php?lvl=notice_display&id=36371
in INTERNATIONAL POLYMER PROCESSING > Vol. 36, N° 3 (2021) . - p. 287-296[article]Réservation
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Code-barres Cote Support Localisation Section Disponibilité 23733 - Périodique Bibliothèque principale Documentaires Disponible Nanofibrous polypeptide hydrogels with collagen-like structure as biomimetic extracellular matrix / Chengkun Zhao in COLLAGEN AND LEATHER, Vol. 5 (2023)
[article]
Titre : Nanofibrous polypeptide hydrogels with collagen-like structure as biomimetic extracellular matrix Type de document : texte imprimé Auteurs : Chengkun Zhao, Auteur ; Xing Li, Auteur ; Shaoquan Bian, Auteur ; Weinan Zeng, Auteur ; Alfredo Ronca, Auteur ; Ugo D'Amora, Auteur ; Maria Grazia Raucci, Auteur ; Jie Liang, Auteur ; Yong Sun, Auteur ; Qing Jiang, Auteur ; Yujiang Fan, Auteur ; Luigi Ambrosio, Auteur ; Xingdong Zhang, Auteur Année de publication : 2023 Article en page(s) : 13 p. Note générale : Bibliogr. Langues : Anglais (eng) Catégories : Caractérisation
Chimie biomimétique
hydrocolloïdes
Matrice extracellulaire
Morphologie (matériaux)
Nanofibres
PolypeptidesUn polypeptide est une chaîne d'acides aminés reliés par des liaisons peptidiques. On parle de polypeptide lorsque la chaîne contient entre 10 et 100 acides aminés. Au-dessus de 100 acides aminés on parle généralement de protéine.
Parmi eux, les peptides multi-cycliques, les peptides phosphorylés ou encore ceux intégrant des liaisons non-peptidiques ou des peptides conjugués.
Certains polypeptides constituent une famille d'antibiotiques dont les molécules très toxiques n'en permettent qu'un usage très limité. D'autres s’imposent aujourd’hui comme des éléments essentiels à la mise au point de vaccins ou de principes actifs destinés aux traitements de certaines pathologies telles que les cancers, les déficiences hormonales, l’ostéoporose.
Rhéologie
Tests de toxicitéIndex. décimale : 547 Chimie organique : classer la biochimie à 574.192 Résumé : Supramolecular peptides exhibit obvious similarities with collagen fibers in terms of self-assembly characteristics, nanofibrous structure, and responsiveness to external stimuli. Here, a series of supramolecular peptides were developed by altering the amino acid sequence, enabling the self-assembly of three types of 4-biphenylacetic acid (BPAA)-tripeptides into fibrous hydrogel through hydrogen bonding and π–π stacking under the influence of ion induction. Transmission electron and scanning electron microscopies revealed that the diameter of the fiber within nanofibrous hydrogels was ~ 10 and ~ 40 nm, respectively, which was similar with the self-assembled collagen fibers. For this reason, these hydrogels could be considered as a biomimetic extracellular substitute. Meanwhile, the gelation concentration induced by ions was even lower than 0.66 wt%, with an elastic modulus of ~ 0.27 kPa, corresponding to a water content of 99.34 wt%. In addition, the three supramolecular hydrogels were found to be good substrates for L929 cell adhesion and MC-3T3 cell proliferation. The overall results implied that BPAA-based hydrogels have a lucrative application potential as cell carriers. Note de contenu : - EXPERIMENTAL SECTION : Materials and methods - The preparation of BPAA-tripeptides - The preparation of BPAA-tripeptides - Hydrogel preparation and morphological characterization - Rheology - CD and fluorescence emission measurements - Cytotoxicity test - BPAA-tripeptides hydrogels co-culture with L929 cells and MC-3T3 cells - ALP staining of BMSCs co-culture with BPAA-tripeptides - Statistics
- RESULTS AND DISCUSSION : The design and optimization of BPAA-tripeptides - The self-assembled nanofibrillar structure of BPAA-tripeptides by changing the sequence of amino acid - Secondary structure and intermolecular interactions analyzed from CD and fluorescence emission spectroscopy - Viscoelastic property of peptides hydrogels through rheological testing - Impact of amino acid sequence change on biological propertiesDOI : https://doi.org/10.1186/s42825-022-00110-6 En ligne : https://link.springer.com/content/pdf/10.1186/s42825-022-00110-6.pdf Format de la ressource électronique : Permalink : https://e-campus.itech.fr/pmb/opac_css/index.php?lvl=notice_display&id=40059
in COLLAGEN AND LEATHER > Vol. 5 (2023) . - 13 p.[article]Nanolatex technology 1 : synthesis and characterization of nanosize acrylic latexes and comparison to their conventional size counterparts / Ravi G. Joshi in JOURNAL OF COATINGS TECHNOLOGY AND RESEARCH, Vol. 18, N° 6 (11/2021)
[article]
Titre : Nanolatex technology 1 : synthesis and characterization of nanosize acrylic latexes and comparison to their conventional size counterparts Type de document : texte imprimé Auteurs : Ravi G. Joshi, Auteur ; Frank N. Jones, Auteur ; Theodore Provder, Auteur ; Weidian Shen, Auteur Année de publication : 2021 Article en page(s) : p. 1481-1500 Note générale : Bibliogr. Langues : Américain (ame) Catégories : Caractérisation
Coalescence (Sciences physiques)
Formation de film
Latex
Microémulsions
Morphologie (matériaux)
Nanoparticules
Polyacryliques
Polymères -- Synthèse
Polymérisation en émulsion
Réticulation (polymérisation)
Revêtements organiquesIndex. décimale : 667.9 Revêtements et enduits Résumé : For this study, functional precoalescence (internally crosslinked) and postcoalescence (crosslinkable) conventional latexes were made using seeded semi-continuous emulsion polymerization. Nanosize polymer latexes with or without crosslinkable functional groups were made using a modified microemulsion copolymerization process. Films cast from conventional and nanosize latex were characterized using specific end use tests and fundamental properties using dynamic mechanical analysis, modulated differential scanning calorimetry, and atomic force microscopy. This study compares conventional and nanosize latex with respect to the effect of the type and level of crosslinking, particle size and distribution on latex film formation and morphology, and end use and fundamental properties. Nanosize latex films in general have superior gloss, solvent resistance, and adhesion but inferior water resistance. Stress–strain Young’s modulus showed an increase as a function of increasing crosslinker level in the nanosize latex films. Note de contenu : - EXPERIMENTAL : Preparation of nanoparticle latexes using improved modified microemulsion copolymerization - Materials - Preparation of conventional size precoalescence or postcoalescence crosslinked conventional latexes
- CHARACTERIZATION OF LATEXES : Latex properties - Film properties of conventional latexes and nanoparticle latexes - Thermal and mechanical properties of conventional latexes and nanoparticle latexes - Measurements with AFM of conventional latexes and nanoparticle latexes
- RESULTS AND DISCUSSIONS : Nanosize latex synthesis and characterization - Film formation by “precoalescence” and “postcoalescence” crosslinked latexes - Gel content results - End-use film properties - Fundamental mechanical properties - Stress–strain analysis of constituent nanosize latexes with precoalescence and postcoalescence crosslinking and comparisons with their conventional size counterparts - Dynamic mechanical properties
- Table 1 : Composition table for nanosize latexes (with or without functional group)
- Table 2 : Characteristics of conventional (with or without crosslinker) latexes
- Table 3 : Characteristics of nanosize (with or without crosslinker) latexes
- Table 4 : End-use properties of films cast from conventional latexes
- Table 5 : End-use properties of films cast from nanosize latexes AFM results
- Table 6 : Comparison of surface smoothness and gloss values of nanoparticle latexes and their conventional counter parts
- Table 7 : Results of stress–strain analysis of nanosize latexes
- Table 8 : Results of stress–strain analysis of conventional size latexes
- Table 9 : Comparison of DMA values with MDSC Tg values of conventionally size precoalescence or postcoalescence crosslinked latexes
- Table 10 : Comparison of DMA values with MDSC Tg values of nanosize precoalescence or postcoalescence crosslinked latexesDOI : https://doi.org/10.1007/s11998-021-00475-z En ligne : https://link.springer.com/content/pdf/10.1007/s11998-021-00475-z.pdf Format de la ressource électronique : Permalink : https://e-campus.itech.fr/pmb/opac_css/index.php?lvl=notice_display&id=36803
in JOURNAL OF COATINGS TECHNOLOGY AND RESEARCH > Vol. 18, N° 6 (11/2021) . - p. 1481-1500[article]Réservation
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Code-barres Cote Support Localisation Section Disponibilité 23146 - Périodique Bibliothèque principale Documentaires Disponible
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Titre : Natural fine-tuning : Blending basalt fibers with plant fibers in thermoplastic and thermoset composites Type de document : texte imprimé Auteurs : Anjum Saleem, Auteur ; Luisa Medina, Auteur Année de publication : 2019 Article en page(s) : p. 45-48 Langues : Anglais (eng) Catégories : Chanvre et constituants Le chanvre ou chanvrier (Cannabis sativa L.) est la seule espèce du genre botanique Cannabis. Ce terme latin est souvent utilisé aussi comme nom vernaculaire pour distinguer les variétés de chanvre cultivé à usage industriel des variétés de cannabis à usage récréatif ou médical. C'est une espèce de plante annuelle, de la famille des Cannabaceae. La graine de chanvre s'appelle le chènevis.
Composites à fibres
Composites à fibres -- Propriétés mécaniques
Composites thermoplastiques
Fibres de basalte
Fibres de basalte -- Propriétés mécaniques
Fibres végétales
Fibres végétales -- Propriétés mécaniques
kénaf et constituantsLe Kenaf (Hibiscus Cannabinus L. et Hibiscus Sabdarifa L.), aussi appelé chanvre de Deccan, est une plante annuelle de la famille des Malvaceae.
Le kenaf est apparenté au jute. Ces tiges épineuses d'1 à 2 cm de diamètre sont souvent, mais pas toujours ramifiée. Les feuilles de 10 à 15 cm de longueur sont de forme variable, celles de la base sont lobées et celles du sommet lancéolées. Les fleurs de 8 à 15 cm de diamètre sont blanches, jaunes ou pourpres. Le fruit est un capsule contenant plusieurs graines.
Lin et constituantsLe lin cultivé (Linum usitatissimum) est une plante annuelle de la famille des Linaceae cultivée principalement pour ses fibres, mais aussi pour ses graines oléagineuses. Les fibres du lin permettent de faire des cordes, du tissu (lin textile pour ses qualités anallergiques, isolantes et thermorégulateurs), ou plus récemment des charges isolantes pour des matériaux de construction. Les graines sont utilisées pour produire de l'huile de lin pour l'industrie de l'encre et de la peinture, pour la consommation humaine et animale, à cause de sa richesse en oméga 3.
Le lin est une des rares fibres textiles végétales européennes. Elle a comme caractéristiques la légereté, la rigidité et la résistance et comme particularité d'être une fibre longue (plusieurs dizaines de centimètres), par rapport aux fibres courtes (coton, chanvre) ou moyennes (laine).
Morphologie (matériaux)
Polyacryliques
Polypropylène
ThermodurcissablesIndex. décimale : 668.4 Plastiques, vinyles Résumé : A blend of natural plant and inorganic fibers produces a composite with a very good property profile, without reducing the content of renewable raw materials. In this way, plant fibers such as kenaf or flax hybridized with basalt fibers can compete with glass fiber reinforcement as a low-cost, natural lightweight construction material. Note de contenu : - Basalt fibers for hybridization of natural plant fibers
- Mechanical characterization of the fibers
- Production of semi-finished products and mechanical characterization of the hybrid
- Morphological characterization
- Processing into components
- Figure : Natural plant and with PP hybridized fiber web after fiber alignment by carding
- Fig. 1 : Comparison of the specific flexural modulus shows that the PP-kenaf composite hybridized with 25% basalt fibers achieves significantly higher values
- Fig. 2 : Specific impact strength of the PP-kneaf composite hybridized with basalt fibers. The addition of 25% basalt fibers increases energy absorption by 45%
- Fig. 3 : Continuous improvement of the specific flexural modulus (stiffness) of the acrylic resin-kenaf/flax composite hybridized with basalt fibers was found with increasing addition of basalt fibers
- Fig. 4 : The scanning electron micrograph of the fracture surface of the PP-KE/BF composite shows pronounced fiber pull-out attributable to a poor fiber-matrix bond
- Fig. 5 : The smooth fibers apparent in the scanning electron micrograph of the fracture surface of the 100% PP-BF composite show that the basalt fiber size used is unsuitable for PP
- Fig. 6 : The scanning electron micrograph of the fracture surface of the acrylic-NF/BF composite shows a homogeneous fracture surface without individually pulled-out fibers
- Fig. 7 : Press molded components made from PP-NF and PP-basalt fibersEn ligne : https://drive.google.com/file/d/18AOtdDjBkEQ6DArNIURPTeyS3d66_8T3/view?usp=drive [...] Format de la ressource électronique : Permalink : https://e-campus.itech.fr/pmb/opac_css/index.php?lvl=notice_display&id=32456
in KUNSTSTOFFE INTERNATIONAL > Vol. 109, N° 4 (04/2019) . - p. 45-48[article]Réservation
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Code-barres Cote Support Localisation Section Disponibilité 20880 - Périodique Bibliothèque principale Documentaires Disponible New biodegradable film produced from cocoa shell nanofibrils containing bioactive compounds / Ozana Almeida Leissa in JOURNAL OF COATINGS TECHNOLOGY AND RESEARCH, Vol. 18, N° 6 (11/2021)
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PermalinkNew liquid crystal polyester filament yarns / Kota Nakamura in CHEMICAL FIBERS INTERNATIONAL, (10/2019)
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