Influence of extrusion conditions on fiber breakage along the srew profile during twin screw compounding of glass fiber-reinforced PA / J. Ville in INTERNATIONAL POLYMER PROCESSING, Vol. XXVIII, N° 1 (03/2013)  

[article]  inINTERNATIONAL POLYMER PROCESSING > Vol. XXVIII, N° 1 (03/2013) . - p. 49-57 Titre : Influence of extrusion conditions on fiber breakage along the srew profile during twin screw compounding of glass fiber-reinforced PA Type de document : texte imprimé Auteurs : J. Ville, Auteur ; F. Inceoglu, Auteur ; N. Ghamri, Auteur ; J. L. Pradel, Auteur ; A. Durin, Auteur ; Rudy Valette, Auteur ; Bruno Vergnes, Auteur Année de publication : 2013 Article en page(s) : p. 49-57 Note générale : Bibliogr. Langues : Anglais (eng) Catégories : Distribution et orientation des fibres Extrudeuse bi-vis Fibres de verre -- Rupture Matériaux hybrides -- Extrusion Polyamide 12 Index. décimale : 668.4 Plastiques, vinyles Résumé : In the present study, Polyamide 12 was compounded with glass fibers in both laboratory and industrial twin screw extruders using various processing conditions (screw speed and feed rate). Dead-stop experiments were performed and samples were collected at different locations along the screws in order to determine the fiber length distribution and the extent of fiber breakage. Results show that significant fiber break-up occurs right after the addition of glass fibers to the molten matrix. Similarly fiber length distribution changes drastically at the first sampling location, near the glass fiber feeder. Processing conditions also influence the extent of degradation: it increases with screw speed and decreases with feed rate, which controls the residence time. Flow modelling has been used to calculate the flow conditions along the screw profile. It is shown that the modified Shon-Liu-White model previously proposed to describe the average fiber length evolution as function of specific energy is not able to correctly predict the evolution along the screw profile. In similar processing conditions, the large industrial extruder appears as less severe than the small laboratory one. Note de contenu : - EXPERIMENTAL : Materials - Fiber length measurements - RESULTS AND DISCUSSION : Laboratory twin screw extruder - Industrial twin screw extruder - Discussion and interpretation DOI : 10.3139/217.2659 En ligne : https://drive.google.com/file/d/146Tw6c-qHGd73ONjlUA89VanYwkZ9Stv/view?usp=drive [...] Format de la ressource électronique : Pdf Permalink : https://e-campus.itech.fr/pmb/opac_css/index.php?lvl=notice_display&id=17764 [article]

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A study of fiber breakage during compounding in a buss kneader / J. Ville in INTERNATIONAL POLYMER PROCESSING, Vol. XXVII, N° 2 (05/2012)  

[article]  inINTERNATIONAL POLYMER PROCESSING > Vol. XXVII, N° 2 (05/2012) . - p. 245-251 Titre : A study of fiber breakage during compounding in a buss kneader Type de document : texte imprimé Auteurs : J. Ville, Auteur ; F. Inceoglu, Auteur ; N. Ghamri, Auteur ; J. L. Pradel, Auteur ; A. Durin, Auteur ; Rudy Valette, Auteur ; Bruno Vergnes, Auteur Année de publication : 2012 Article en page(s) : p. 245-251 Note générale : Bibliogr. Langues : Anglais (eng) Catégories : Composites à fibres de verre Fibres de verre -- Rupture Malaxeurs et mélangeurs Polyamides Un polyamide est un polymère contenant des fonctions amides -C(=O)-NH- résultant d'une réaction de polycondensation entre les fonctions acide carboxylique et amine. Selon la composition de leur chaîne squelettique, les polyamides sont classés en aliphatiques, semi-aromatiques et aromatiques. Selon le type d'unités répétitives, les polyamides peuvent être des homopolymères ou des copolymères. Index. décimale : 668.9 Polymères Résumé : This paper is devoted to the study of fiber breakage during compounding with a polyamide matrix in a Buss kneader. Results showed a drastic decrease of glass fiber length during compounding, typically from 3 500 to 350 µm. Fiber breakage depended on processing conditions: it increased with screw speed, but the effect of feed rate was less clear. Fiber breakage increased also with the severity of the screw profile. Characterizations of fiber length evolution along the screw profile have also been performed after dead-stop experiments. Generally speaking, fiber length evolution can be described using a modified Shon-Liu-White model, in which either the number of turns or the specific energy is considered. Note de contenu : - EXPERIMENTAL : Materials - Compouding procedure - Morphological characterization - RESULTS AND DISCUSSION : Processing parameters - Evolution of fiber lengths with processing conditions - Evolution of fiber lengths along the screw DOI : 10.3139/217.2525 En ligne : https://drive.google.com/file/d/10KvG58M4F9d3a_QanMT6qoQTSWqks3m7/view?usp=drive [...] Format de la ressource électronique : Pdf Permalink : https://e-campus.itech.fr/pmb/opac_css/index.php?lvl=notice_display&id=14694 [article]

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