Preparation and characterization of a biocomposite based on cork microparticles in poly(B-hydroxybutyrate)-co-poly(B-hydroxyvalerate) matrix / Mariem Ayadi in INTERNATIONAL POLYMER PROCESSING, Vol. XXXIV, N° 2 (05/2019)  

[article]  inINTERNATIONAL POLYMER PROCESSING > Vol. XXXIV, N° 2 (05/2019) . - p. 270-278 Titre : Preparation and characterization of a biocomposite based on cork microparticles in poly(B-hydroxybutyrate)-co-poly(B-hydroxyvalerate) matrix Type de document : texte imprimé Auteurs : Mariem Ayadi, Auteur ; R. Ben Cheikh, Auteur ; N. Dencheva, Auteur ; Z. Denchev, Auteur Année de publication : 2019 Article en page(s) : p. 270-278 Note générale : Bibliogr. Langues : Anglais (eng) Catégories : Allongement à la rupture Charges (matériaux) Composites -- Moulage par compression Composites -- Propriétés mécaniques Composites -- Propriétés thermiques Copolymères Elasticité Essais dynamiques Liège Matériaux hybrides Particules (matières) Poly-B-hydroxybutyrate poly-B-hydroxyvalérate Traction (mécanique) Index. décimale : 668.4 Plastiques, vinyles Résumé : Poly(β-hydroxybutyrate)-co-poly(β-hydroxyvalerate) (PHBV) loaded with 1 to 10 wt.% of cork microparticles (CM) were manufactured via compression molding technique. CM were isolated by alkali, bleaching and acid hydrolysis treatments. They were then added to the PHBV matrices via solution casting technique. The filler microparticles showed typical diameters of 10 to 55 μm. Mechanical tests in tension showed that in PHBV containing 5 wt.% CM the Young's modulus and the tensile strength increased by 50% and 10% respectively. Meanwhile, the elongation at break decreased by 70% for the same CM content. The mechanical behavior of the reinforced composites was discussed in conjunction with the morphology of the samples studied by optical and electron microscopy. The temperature of initial degradation Tid, the temperature at 5% weight loss Td5% and the temperature of maximum degradation Tdmax increase with increasing CM content by up to 13.6°C, 10.1°C and 12.3°C respectively for the composite of 5 wt.%. The composite with 10 wt.% CM content showed the best thermal stability with temperature increments of 20°C, 14.1°C and 21.5°C respectively. DSC results showed that the presence of CM has a very weak influence on the melting/crystallization behavior of the composites. Note de contenu : - EXPERIMENTAL : Materials - Isolation of cork microparticles - Preparation of the PHBV/CM composites - Characterization - RESULTS AND DISCUSSION : Morphological studies by microscopy - Thermal stability - Melting and crystallization behavior - Mechanical properties DOI : 10.3139/217.3713 En ligne : https://drive.google.com/file/d/11v7IpsHwHZK8xpGqrjvl7LkO-l6rQZjU/view?usp=drive [...] Format de la ressource électronique : Pdf Permalink : https://e-campus.itech.fr/pmb/opac_css/index.php?lvl=notice_display&id=32403 [article]

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