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Applications of X-ray diffraction and fluorescence techniques in coatings industries / G. Bathiri in PAINTINDIA, Vol. LI, N° 9 (09/2001)
[article]
Titre : Applications of X-ray diffraction and fluorescence techniques in coatings industries Type de document : texte imprimé Auteurs : G. Bathiri, Auteur Année de publication : 2001 Article en page(s) : p. 33-40 Note générale : Bibliogr. Langues : Anglais (eng) Tags : 'Matériau revêtement' Peinture Feuil 'Analyse chimique' Pigment quantitative' qualitative' 'Détection défaut' Cristallinité surface' 'Diffraction RX' 'Spectrométrie fluorescence Index. décimale : 667.9 Revêtements et enduits Résumé : X-ray diffraction spectroscopy (XRD) and X-ray fluorescence spectroscopy (XRF) are very useful techniques in the characterisation of materials. In XRD, the angle of diffraction of X-ray is measured after allowing X-rays to be incident on the material under testing. The distance between layer of atoms (d) then can be calculated using Bragg's equation. Plot of intensity vs d - value gives XRD spectrum. In XRF, X-rays of high wavelength are emitted by the specimen as a result of transition of electrons between orbitals when bombarded by low wavelength X-rays. XRF spectrum is a plot of intensity as a function of either energy or wavelength. XRD & XRF spectra are characteristics of materials and form the basis of their analysis. In coatings XRD is useful in establishing the identity and determining the purity of pigments. The technique is useful for analysis of polymorphic forms in titanium dioxides (rutile and anatase) and copper phthalocyanines (alpha, beta and gamma). XRD has also been used in the determination of identity and amount of pretreatment on metal or in general, crystalline coatings on substrate. XRD also finds use in identifying coating defects. XRF can act as a supporting tool to XRD and can be useful in determination of various elements used in coatings in wider range from ppm to 100%. Both XRD and XRF are useful in coating industry as research, quality control and problem analysis tool. Although these techniques are expensive, their simplicity of operations, speed and ability to give selective information make them a very powerful analytical tool for study of coatings. Note de contenu : - INSTRUMENTATION FOR X-RAY TECHNIQUES
- X-RAY DIFFRACTION : Bragg's law
- APPLICATIONS OF X-RAY DIFFRACTION ANALYSIS : Identification of pigments - Quantitative analysis of pigment mixtures - Determination of anatase TiO2 content in rutile TiO2 - Study of polymorphism - Use of XRD for tracking coating defect - Characterisation of metal pretreatment and other thin coatings - Crystallinity of polymers - Particle size - Monitoring of chemical reactions.
- X-RAY FLUORESCENCE SPECTROSCOPY : Qualitative analysis - Quantitative anlaysis
- APPLICATIONS OF X-RAY FLUORESCENCE SPECTROMETRY : Support for X-ray diffraction analysis - Analysis of elements in solution - Quality control
- ADVANTAGES AND DISADVANTAGES OF XRFPermalink : https://e-campus.itech.fr/pmb/opac_css/index.php?lvl=notice_display&id=12457
in PAINTINDIA > Vol. LI, N° 9 (09/2001) . - p. 33-40[article]Réservation
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Code-barres Cote Support Localisation Section Disponibilité 001270 - Périodique Bibliothèque principale Documentaires Disponible Thermoplastic powder coatings : Correlating thermal history and performance / Shelby F. Thames in EUROPEAN COATINGS JOURNAL (ECJ), N° 10/95 (10/1995)
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Titre : Thermoplastic powder coatings : Correlating thermal history and performance Type de document : texte imprimé Auteurs : Shelby F. Thames, Auteur ; Kamlesh G. Panjnani, Auteur ; Samuel D. Pace, Auteur Année de publication : 1995 Article en page(s) : p. 692-693 Note générale : Bibliogr. Langues : Anglais (eng) Catégories : Revêtements poudre:Peinture poudre
ThermoplastiquesUne matière thermoplastique désigne une matière qui se ramollit (parfois on observe une fusion franche) d'une façon répétée lorsqu'elle est chauffée au-dessus d'une certaine température, mais qui, au-dessous, redevient dure. Une telle matière conservera donc toujours de manière réversible sa thermoplasticité initiale. Cette qualité rend le matériau thermoplastique potentiellement recyclable (après broyage). Cela implique que la matière ramollie ne soit pas thermiquement dégradée et que les contraintes mécaniques de cisaillement introduites par un procédé de mise en forme ne modifient pas la structure moléculaire.Tags : 'Peinture poudre' Thermoplastique 'Amide 11 polymère' 12 'Vinylique alcool copolymère' acétate 'Ethylène 'Vinylidène fluorure 'Etude expérimentale' 'Calorimétrie différentielle balayage' 'Diffraction RX' 'Traitement thermique' Trempe Recuit 'Propriété mécanique' Feuil Index. décimale : 667.9 Revêtements et enduits Résumé : This study examines thermoplastic polyamide 11, nylon 12, ethylenevinylacetate/vinylalcohol copolymer, poly (vinylidene fluoride), and polyester powder coatings via differential scanning calorimetry and wide angle x-ray diffraction studies to quantify annealing and quenching effects. As a part of this study, panels were coated and cured at 250°C for 5 min. Cooling was affected by either rapid quenching or controlled annealing. The thermal, mechanical, and x-ray diffraction analysis data indicate no significant property changes on quenching or annealing the thermoplastic coatings with the exception of the highly crystalline poly (vinylidene fluoride) coating. Annealing the latter coating reduced impact resistance and flexibility. These findings are consistent with earlier results in which no major stress development was observed in quenched thermosetting powder coatings, yet annealing increased crosslink density and diminished mechanical properties. Permalink : https://e-campus.itech.fr/pmb/opac_css/index.php?lvl=notice_display&id=11365
in EUROPEAN COATINGS JOURNAL (ECJ) > N° 10/95 (10/1995) . - p. 692-693[article]Réservation
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Code-barres Cote Support Localisation Section Disponibilité 002508 - Périodique Bibliothèque principale Documentaires Disponible 002509 - Périodique Bibliothèque principale Documentaires Disponible