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Silylated linseed oil - invisible wood protection ? / Ewelina Depczynska in SURFACE COATINGS INTERNATIONAL, Vol. 102.1 (02-03/2019)
[article]
Titre : Silylated linseed oil - invisible wood protection ? Type de document : texte imprimé Auteurs : Ewelina Depczynska, Auteur ; Monika Furgal, Auteur ; Bartlomiej Mazela, Auteur ; Waldemar Perdoch, Auteur Année de publication : 2019 Article en page(s) : p. 22-26 Note générale : Bibliogr. Langues : Anglais (eng) Catégories : Biopolymères
Bois -- Revêtements protecteurs
Caractérisation
Chimie analytique
Huile de linL'huile de lin ou "huile de graines de lin" est une huile de couleur jaune d'or, tirée des graines mûres du lin cultivé, pressées à froid et/ou à chaud ; parfois elle est extraite par un solvant, en vue de l'usage industriel ou artistique, principalement comme siccatif, ou huile auto-siccative.
Les utilisations de l'huile de lin dérivent de sa richesse en acides gras polyinsaturés, en particulier en acides linolénique et linoléique, qui lui doivent leur nom.
L'huile de lin polymérise spontanément à l'air, avec une réaction exothermique : un chiffon imbibé d'huile peut ainsi, dans certaines conditions, s'enflammer spontanément.
Pour ses propriétés de polymère, l'huile de lin est employée seule, ou mélangée à d'autres huiles, résines et solvants, et est utilisée en tant que : Imprégnateur et protecteur des bois à l'intérieur comme à l'extérieur : protection contre l'humidité, les champignons et insectes, et contre la poussière par son caractère antistatique, composant de certains vernis de finition, liant de broyage pour la peinture à l'huile, agent plastifiant du mastic de vitrier, agent durcisseur de diverses préparations, agent de cohérence et liant dans la fabrication du linoléum.
Hydrophobie
SilylationLa silylation est l'introduction d'un groupe silyle, généralement substitué (R3Si–), dans une molécule.
ViscositéIndex. décimale : 667.9 Revêtements et enduits Résumé : Synthesis of a non-film forming product for wood protection based on silylated linseed oil with the objective of obtaining an innovative oil-based product for superficial wood treatment with a permanent hydrophobic effect is described. Product containing different molar ratios of oil and silane were synthesised and characterised. The goals were to monitor the silylation process with the use of VTMOS and to evaluate some of the physico-chemical properties of the polymers obtained. The structures of the new polymers were determined by 1H and 13C NMR spectroscopy and selected physico-chemical properties (eg. iodine value, viscosity) were also determined. The results show that the modified oil is storagestable and its basic functional properties in a liquid state are comparable with reference products. Physical porperty data indicates that the resultant bio-based polymers are suitable for wood treatment as non-film forming products. Note de contenu : - Materials
- Methods
- Characterisation of silylated linseed oil
- Fig. 1 : Chemical composition of the most commonly used natural oils in wood preservatives
- Fig. 2 : Variation of pressure with time during silylation of linseed oil
- Fig. 3 : Variation of pressure with time during silylation of linseed oil
- Table 1 : Reaction mixture composition and time of silylation reaction
- Table 2 : Viscosity of reactants and products in the silylation of linseed oil
- Table 3 : GC-FID analysis for reactants and products in selected silylation reactions
- Table 4 : Iodine values for selected reactions
- Table 5 : Chemical shifts (δ) and assignment of main resonances in the 1H NMR spectrum of raw linseed oil
- Table 6 : Chemical shifts (δ) and assignment of main resonances in the 1H NRM spectrum from product of reaction 1
- Table 7 : Chemical shifts (δ) and assignment of main resonances in the 1H NRM spectrum of reaction 9 and VTMS
- Table 8 : Chemical shifts (δ) and assignment of main resonances in the 13C NRM spectrum of raw linseed oil
- Table 9 : Chemical shifts (δ) and assignment of main resonances in the 13C NRM spectrum from product of reaction 9
- Table 10 : Chemical shifts (δ) and assignment of main resonances in the 13C NRM spectrum from product of reaction 1
- Table 11 : UV-VIS absorption (λ) 385 nm) for linseed oil and products from selected reactionsEn ligne : https://drive.google.com/file/d/1ZQUjYsZ0xrI03_r8Ie23-oTAidM1ck0j/view?usp=drive [...] Format de la ressource électronique : Permalink : https://e-campus.itech.fr/pmb/opac_css/index.php?lvl=notice_display&id=32021
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Code-barres Cote Support Localisation Section Disponibilité 20740 - Périodique Bibliothèque principale Documentaires Disponible A simple and cost-effective method for fabricating lotus-effect composite coatings / Changhong Su in JOURNAL OF COATINGS TECHNOLOGY AND RESEARCH, Vol. 9, N° 2 (03/2012)
[article]
Titre : A simple and cost-effective method for fabricating lotus-effect composite coatings Type de document : texte imprimé Auteurs : Changhong Su, Auteur Année de publication : 2012 Article en page(s) : p. 135-141 Note générale : Bibliogr. Langues : Américain (ame) Catégories : Angle de contact
Angle de glissement
Composites
Epoxydes
Hydrophobie
Nanoparticules
Particules (matières)
Revêtements:Peinture
SiliceLa silice est la forme naturelle du dioxyde de silicium (SiO2) qui entre dans la composition de nombreux minéraux.
La silice existe à l'état libre sous différentes formes cristallines ou amorphes et à l'état combiné dans les silicates, les groupes SiO2 étant alors liés à d'autres atomes (Al : Aluminium, Fe : Fer, Mg : Magnésium, Ca : Calcium, Na : Sodium, K : Potassium...).
Les silicates sont les constituants principaux du manteau et de l'écorce terrestre. La silice libre est également très abondante dans la nature, sous forme de quartz, de calcédoine et de terre de diatomée. La silice représente 60,6 % de la masse de la croûte terrestre continentale.Index. décimale : 667.9 Revêtements et enduits Résumé : This paper reports the fabrication of a lotus-effect coating by grafting epoxy (EP) resin on the surface of microsilica and nanosilica, respectively, and subsequent spraying. The coating shows the same structure and capability as lotus leaves, and shows a static contact angle as large as 165° and a sliding angle as small as 2.5°. SEM analysis shows that the hydrophobic capability depends on the surface structure of the coatings. This method may be suited for processing large scale or irregular surfaces. Note de contenu : - EXPERIMENTAL : Materials and chemicals - Preparation of the EP solution - Fabrication of lotus-effect coatings - Measurement
- RESULTS AND DISCUSSION : Preparation of dual-sized surfaces - Static CA and SA - Surface morphology - Chemical elements of the surface - Discussion of the relationship between hydrophobic ability and surface morphologyDOI : 10.1007/s11998-009-9230-0 En ligne : https://link.springer.com/content/pdf/10.1007/s11998-009-9230-0.pdf?pdf=button Format de la ressource électronique : Permalink : https://e-campus.itech.fr/pmb/opac_css/index.php?lvl=notice_display&id=14363
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Code-barres Cote Support Localisation Section Disponibilité 14096 - Périodique Bibliothèque principale Documentaires Disponible A simple method for the fabrication of silica-based superhydrophobic surfaces / Qianqian Shang in JOURNAL OF COATINGS TECHNOLOGY AND RESEARCH, Vol. 11, N° 4 (07/2014)
[article]
Titre : A simple method for the fabrication of silica-based superhydrophobic surfaces Type de document : texte imprimé Auteurs : Qianqian Shang, Auteur ; Yonghong Zhou, Auteur ; Guomin Xiao, Auteur Année de publication : 2014 Article en page(s) : p. 509-515 Note générale : Bibliogr. Langues : Américain (ame) Catégories : Angle de contact
Caractérisation
Dépôt par pulvérisation
Hydrophobie
Particules (matières)
Revêtements protecteurs
Revêtements:Peinture
SiliceLa silice est la forme naturelle du dioxyde de silicium (SiO2) qui entre dans la composition de nombreux minéraux.
La silice existe à l'état libre sous différentes formes cristallines ou amorphes et à l'état combiné dans les silicates, les groupes SiO2 étant alors liés à d'autres atomes (Al : Aluminium, Fe : Fer, Mg : Magnésium, Ca : Calcium, Na : Sodium, K : Potassium...).
Les silicates sont les constituants principaux du manteau et de l'écorce terrestre. La silice libre est également très abondante dans la nature, sous forme de quartz, de calcédoine et de terre de diatomée. La silice représente 60,6 % de la masse de la croûte terrestre continentale.Index. décimale : 667.9 Revêtements et enduits Résumé : The present article reports on a simple and convenient method for the fabrication of superhydrophobic surfaces based on silica particles by spraying the as-prepared silica suspension containing silica sol and silica microspheres on the substrate. The morphologies of the silica particulate coatings could be controlled by varying the silica microsphere concentration. The silica particulate coatings as prepared were exceptionally rough and superhydrophilic, with water contact angles less than 5°. The surface silanol groups of the hydrophilic coatings could be functionalized using 1H,1H,2H,2H-perfluorodecyltriethoxysilane to form hydrophobic groups. The resulting surface showed excellent superhydrophobic property with water contact angle up to 165.6 ± 0.9° and sliding angle of 3.5 ± 0.4°. In addition, the superhydrophobicity of the coating possessed a good stability after 3 months of exposure in air for a wide range of pH values. Note de contenu : - Materials
- Fabrication of the silica particulate coatings
- CharacterizationsDOI : 10.1007/s11998-014-9573-z En ligne : https://link.springer.com/content/pdf/10.1007%2Fs11998-014-9573-z.pdf Format de la ressource électronique : Permalink : https://e-campus.itech.fr/pmb/opac_css/index.php?lvl=notice_display&id=21712
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Code-barres Cote Support Localisation Section Disponibilité 16424 - Périodique Bibliothèque principale Documentaires Disponible A simple method to make mechanically robust, adhesive and superhydrophobic surface based on epoxy resin / Aoyun Zhuang in JOURNAL OF COATINGS TECHNOLOGY AND RESEARCH, Vol. 12, N° 3 (05/2015)
[article]
Titre : A simple method to make mechanically robust, adhesive and superhydrophobic surface based on epoxy resin Type de document : texte imprimé Auteurs : Aoyun Zhuang, Auteur ; Lijun Yang, Auteur ; Ruijin Liao, Auteur ; Chao Guo, Auteur ; Zhiping Zuo, Auteur ; Yuan Yuan, Auteur Année de publication : 2015 Article en page(s) : p. 609-615 Note générale : Bibliogr. Langues : Américain (ame) Catégories : Abrasion
Adhésifs -- Propriétés mécaniques
Bisphénol A
Caractérisation
Colles:Adhésifs
Epoxydes
Essais dynamiques
Hydrophobie
Nanoparticules
Résistance chimique
SiliceLa silice est la forme naturelle du dioxyde de silicium (SiO2) qui entre dans la composition de nombreux minéraux.
La silice existe à l'état libre sous différentes formes cristallines ou amorphes et à l'état combiné dans les silicates, les groupes SiO2 étant alors liés à d'autres atomes (Al : Aluminium, Fe : Fer, Mg : Magnésium, Ca : Calcium, Na : Sodium, K : Potassium...).
Les silicates sont les constituants principaux du manteau et de l'écorce terrestre. La silice libre est également très abondante dans la nature, sous forme de quartz, de calcédoine et de terre de diatomée. La silice représente 60,6 % de la masse de la croûte terrestre continentale.
Verre -- CollageIndex. décimale : 667.9 Revêtements et enduits Résumé : A robust micro/nano-structured superhydrophobic surface was facilely prepared by applying composite coating consisting of epoxy resin and silica nanoparticles on glass substrates. The whole process only needed bisphenol A-based epoxy resin and silica nanoparticles to be mixed, coated, and dried. Field emission scanning electron microscopy, atomic force microscopy, and a drop meter were utilized to evaluate its morphology, accurate topography, quantitative roughness, and wettability, respectively. After considering adhesive force and the superhydrophobicity of the coating, it was shown that the best result was gained when the solid content of the silica nanoparticles was 45.5 wt%. In addition, the coating showed excellent surface mechanical stability and acid-alkali resistance which offers great potential for durable application in various fields. Note de contenu : - EXPERIMENT : Materials - Preparation of superhydrophobic epoxy resin surface - Characterization of samples
- RESULTS AND DISCUSSION : Superhydrophobic surfaces from bisphenol A epoxy with silica nanoparticles - Abrasion test for robust structure - Test of acid-alkali resistance of superhydrophobic surfacesDOI : 10.1007/s11998-014-9653-0 En ligne : https://link.springer.com/content/pdf/10.1007%2Fs11998-014-9653-0.pdf Format de la ressource électronique : Permalink : https://e-campus.itech.fr/pmb/opac_css/index.php?lvl=notice_display&id=24185
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Code-barres Cote Support Localisation Section Disponibilité 17244 - Périodique Bibliothèque principale Documentaires Disponible Slippery lubricant-infused intertwining superhydrophobic matrix: preparation and enhanced resistance against abiotic corrosion and microbiologically influenced corrosion / Yinsha Wei in JOURNAL OF COATINGS TECHNOLOGY AND RESEARCH, Vol. 20, N° 2 (03/2023)
[article]
Titre : Slippery lubricant-infused intertwining superhydrophobic matrix: preparation and enhanced resistance against abiotic corrosion and microbiologically influenced corrosion Type de document : texte imprimé Auteurs : Yinsha Wei, Auteur ; Yizhen Yu, Auteur ; Yunxiang Wang, Auteur ; Yuekun Jing, Auteur ; Hongge Gao, Auteur ; Bingzhi Li, Auteur ; Shugang Hu, Auteur ; Ri Qiu, Auteur ; Yibo Ouyang, Auteur Année de publication : 2023 Article en page(s) : p. 647-660 Note générale : Bibliogr. Langues : Américain (ame) Catégories : Acier au carbone
Anticorrosifs
Anticorrosion
Caractérisation
Chimie biomimétique
Corrosion
Essais de brouillard salin
Hydrophobie
Lubrifiants
Métaux -- Revêtements protecteurs
SiliconesLes silicones, ou polysiloxanes, sont des composés inorganiques formés d'une chaine silicium-oxygène (...-Si-O-Si-O-Si-O-...) sur laquelle des groupes se fixent, sur les atomes de silicium. Certains groupes organiques peuvent être utilisés pour relier entre elles plusieurs de ces chaines (...-Si-O-...). Le type le plus courant est le poly(diméthylsiloxane) linéaire ou PDMS. Le second groupe en importance de matériaux en silicone est celui des résines de silicone, formées par des oligosiloxanes ramifiés ou en forme de cage (wiki).Index. décimale : 667.9 Revêtements et enduits Résumé : The corrosion of carbon steel (CS) is a disastrous threat to artificial engineering in harsh environments, such as underground mines and seawater environments. Herein, we employed facile one-step electrodeposition to prepare a superhydrophobic intertwining structure on a CS surface in an effort to alleviate corrosion. Sophisticated characterization methods suggested that La tetradecanoate formed during the electrodeposition process via an electrochemical reduction reaction. Silicone lubricant acted as the insoluble phase and was infused into the superhydrophobic matrix to yield a biomimetic slippery lubricant-infused surface (LIS) due to the capillary effect from the superhydrophobic intertwining structure to the lubricant phase. Using natural seawater, salt spray and sulfate-reducing bacteria (SRB) suspension as the harsh media, LIS shows excellent corrosion resistance to the underlying metal compared with bare CS and the superhydrophobic surface covering CS because the oil phase acts as a barrier to inhibit the penetration of corrosive species. For the LIS sample after seawater immersion for 20 d, the Icorr was approximately 2 orders of magnitude smaller than that of the bare CS. In addition, after a 5.0 wt% salt spray test for 20 d, the |Z|0.01 Hz of the LIS surface was ca. 3 orders of magnitude larger than that of CS. Furthermore, when immersed in an extremely harsh SRB suspension for 15 d, the |Z|0.01 Hz of LIS was ca. 3 orders of magnitude larger than that of bare CS because LIS can dually prohibit the bioattachment of SRB and avoid the penetration of the highly corrosive metabolite. Thus, the LIS was proven to have prominent anticorrosion properties in harsh corrosive environments. Note de contenu : - Preparation of SHS and LIS onto CS
- Morphology, composition and wettability characterization
- Corrosion inhibition measurement in different environments
- Evaluation of bio-attachment and corrosion inhibition of the coatings in sulfate-reducing bacteria (SRB) suspension
- Table 1 : The electrochemical parameters of bare CS, SHS and LIS revealed by potentiodynamic polarization curves during immersion in seawater
- Table 2 : The electrochemical parameters of CS and LIS were revealed by potentiodynamic polarization curves after exposure to 5.0 wt% salt spray for certain periods
- Table 3 : The electrochemical parameters of CS and LIS were revealed by potentiodynamic polarization after being immersed in the SRB suspension for certain periodsDOI : https://doi.org/10.1007/s11998-022-00698-8 En ligne : https://link.springer.com/content/pdf/10.1007/s11998-022-00698-8.pdf?pdf=button% [...] Format de la ressource électronique : Permalink : https://e-campus.itech.fr/pmb/opac_css/index.php?lvl=notice_display&id=39309
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Code-barres Cote Support Localisation Section Disponibilité 24056 - Périodique Bibliothèque principale Documentaires Disponible PermalinkSodium silicate-assisted emulsification of methyltrimethoxysilane and formation of superhydrophobic coating thereof / Ying Wang in JOURNAL OF COATINGS TECHNOLOGY AND RESEARCH, Vol. 12, N° 4 (07/2015)
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