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On-line determination of sulphide in tannery effluent by flow injection analysis / Yu Lan in JOURNAL OF THE SOCIETY OF LEATHER TECHNOLOGISTS & CHEMISTS (JSLTC), Vol. 96, N° 6 (11-12/2012)
[article]
Titre : On-line determination of sulphide in tannery effluent by flow injection analysis Type de document : texte imprimé Auteurs : Yu Lan, Auteur ; Yu Lingyun, Auteur ; Zhang Xinshen, Auteur Année de publication : 2012 Article en page(s) : p. 256-260 Note générale : Bibliogr. Langues : Anglais (eng) Catégories : Absorption
AlizarineL'alizarine est un colorant rouge d'origine végétale, extrait de la racine de la garance des teinturiers (Rubia tinctorum L.), une plante vivace de la famille des Rubiacées, autrefois largement cultivée pour la teinture qu'elle fournissait.
Eaux usées -- Analyse
Eaux usées -- Teneur en ions sulfures
SpectrophotométrieIndex. décimale : 675 Technologie du cuir et de la fourrure Résumé : A simple and rapid spectrophotometric method for the determination of sulphide has been developed using flow injection analysis. The proposed method is based on the reducibility of sulphide ion towards alizarin red S resulting in an intense red complex with a suitable absorption peak at 515nm. The absorbance value of this compound is directly proportional to the concentration. Optimum conditions for determining sulphide were investigated by a univariate method. Under the optimum conditions for determining sulphide were investigated by a univariate method. Under the optimum conditions a linear calibration graph was obtained over the range 0.01-4.0mg l-1, the detection limit was 4.0µg l-1, the relative standard deviation was 1.04% (n=13) and the standard addition recovery was between 103.7 % and 106.0%. The method has been statisfactorily applied for the determination of sulphide in tannery effluents. Note de contenu : - EXPERIMENTAL PROCEDURES : Reagents and solutions - Apparatus - Recommended procedure
- RESULTS AND DISCUSSION : Choice of the detection wavelength - Preliminary investigation - Method validationEn ligne : https://drive.google.com/file/d/1XPjHGxfqxtejEazRX9Sa4CIg11o9T41n/view?usp=drive [...] Format de la ressource électronique : Permalink : https://e-campus.itech.fr/pmb/opac_css/index.php?lvl=notice_display&id=16810
in JOURNAL OF THE SOCIETY OF LEATHER TECHNOLOGISTS & CHEMISTS (JSLTC) > Vol. 96, N° 6 (11-12/2012) . - p. 256-260[article]Réservation
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Code-barres Cote Support Localisation Section Disponibilité 14414 - Périodique Bibliothèque principale Documentaires Disponible Rapid determination of sulphide in tannery wastewater by spectrophotometry / Chen Shujuan in JOURNAL OF THE SOCIETY OF LEATHER TECHNOLOGISTS & CHEMISTS (JSLTC), Vol. 95, N° 3 (05-06/2011)
[article]
Titre : Rapid determination of sulphide in tannery wastewater by spectrophotometry Type de document : texte imprimé Auteurs : Chen Shujuan, Auteur ; Zhang Xinshen, Auteur ; Yu Lingyun, Auteur ; Cao Fengmei, Auteur ; Zhao Huanhuan, Auteur ; Li Hui, Auteur Année de publication : 2011 Article en page(s) : p. 121-125 Note générale : Bibliogr. Langues : Anglais (eng) Catégories : Eaux usées -- Teneur en ions sulfures
Molybdène
Réduction (chimie)
Silicium
Spectrophotométrie
TannageIndex. décimale : 675.2 Préparation du cuir naturel. Tannage Résumé : A simple and rapid spectrophotometric flow injection analysis method for the determination of sulphide has been developed. The proposed method was based on the reducibility of sulphide ion by silicon-molybdenum heteropoly acid, resulting in an intense blue complex with absorption at 630nm. The absorbance value of this compound is directly proportional to the concentration. Optimum conditions for determining sulphide were investigated by a univariate method. Under the optimum conditions, a linear calibration graph was obtained over the range 0-200mg l-1, the detection limit was 32.8µg l-1, the relative standard deviation was 1.86 % (n=12) and the standard addition recovery was between 96.12 % and 104.50 %. The method has been satisfactorily applied for the determination of sulphide in tannery wastewater samples. Note de contenu : EXPERIMENTAL PROCEDURES : Reagents and solutions - Apparatus - Recommended procedure.
RESULTS AND DISCUSSION : Preliminary investigation - Optimization of colour solution (R) - Effect of reaction coil length - Effect of sampling volume - Method validation.En ligne : https://drive.google.com/file/d/1aAX9vAx-xk80UuOU1dsoJ7MPfmSLGUif/view?usp=drive [...] Format de la ressource électronique : Permalink : https://e-campus.itech.fr/pmb/opac_css/index.php?lvl=notice_display&id=11881
in JOURNAL OF THE SOCIETY OF LEATHER TECHNOLOGISTS & CHEMISTS (JSLTC) > Vol. 95, N° 3 (05-06/2011) . - p. 121-125[article]Réservation
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Code-barres Cote Support Localisation Section Disponibilité 013132 - Périodique Bibliothèque principale Documentaires Disponible