| Titre : |
Polyvinylidene fluoride/maghnite nanocomposites : fabrication and study of structural, thermal and mechanical properties |
| Type de document : |
texte imprimé |
| Auteurs : |
Zoulikha Khiati, Auteur ; Lahouari Mrah, Auteur |
| Année de publication : |
2023 |
| Article en page(s) : |
p. 615-624 |
| Note générale : |
Bibliogr. |
| Langues : |
Anglais (eng) |
| Catégories : |
Analyse mécanique dynamique
Analyse thermique
Caractérisation
Matériaux hybrides
Matériaux hybrides -- Propriétés mécaniques
Polyfluorure de vinylidène
Viscosité
|
| Index. décimale : |
668.4 Plastiques, vinyles |
| Résumé : |
An in-depth study of polyvinylidene fluoride (PVDF) based nanocomposite systems will be the focus of this research. This polymer being hydrophobic and apolar, it will be unlikely to generate strong interactions with clay leaves called organophilic maghnite. The challenge of this study will therefore be to manage the load/polymer interfaces by using montmorillonite with specific surface treatments by adding a surfactant Cetyltrimethylammonium bromide. Therefore, a significant improvement in mechanical and thermal properties was observed. The properties of PVDFNC nanocomposites were evaluated using various physico-chemical techniques (XRD, FTIR, TGA, DSC, TEM, SEM). The results of the structural and thermal measurements carried out on these products reveal that the structural concept of the surfactant influences both the morphological profile, the thermal and mechanical properties of the nanocomposites obtained. Accelerated crystallization is observed in PVDNC nanocomposites as an effective nucleation agent, the crystals formed are predominantly β shaped and have a small number of polar α crystals. Measurements by X-ray diffraction, as well as transmission and scanning electron microscopy indicated that modified maghnite was perfectly distributed 3 % by weight in the polyvinylidene fluoride matrix. The mechanical properties of the nanocomposites were evaluated according to the filler material used and the polyvinylidene fluoride matrix. |
| Note de contenu : |
- MATERIALS AND METHODS : Materials - Preparation of PVDFN nanocomposites - Characterization
- RESULTS AND DISCUSSION : FTIR analysis - X-ray diffraction analysis - Transmission electron microscopy analysis - Scanning electron microscopy analysis - Optical microscopy - Thermogravimetric analysis - DSC - Index of fluidity (IF) - Dynamic mechanical thermal analysis (DMTA) - Mechanical properties
- Table 1 : The mechanical properties of the polymer PVDF and its nanocomposites |
| DOI : |
https://doi.org/10.1515/ipp-2022-4302 |
| En ligne : |
https://drive.google.com/file/d/1HzmeWpX0XDfyOG9B3TOQk7Aygdcr1R30/view?usp=drive [...] |
| Format de la ressource électronique : |
Pdf |
| Permalink : |
https://e-campus.itech.fr/pmb/opac_css/index.php?lvl=notice_display&id=40293 |
in INTERNATIONAL POLYMER PROCESSING > Vol. 38, N° 5 (2023) . - p. 615-624
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