Biosurfactant in planar chromatography of transition metal ions : mixed micelles activated separations / A. Moheman in TENSIDE, SURFACTANTS, DETERGENTS, Vol. 48, N° 4/2011 (07-08/2011)

[article]  inTENSIDE, SURFACTANTS, DETERGENTS > Vol. 48, N° 4/2011 (07-08/2011) . - p. 275-280 Titre : Biosurfactant in planar chromatography of transition metal ions : mixed micelles activated separations Type de document : texte imprimé Auteurs : A. Moheman, Auteur ; A. Husain, Auteur ; K. S. Siddiqi, Auteur Année de publication : 2011 Article en page(s) : p. 275-280 Note générale : Bibliogr. Langues : Anglais (eng) Catégories : Surfactants Tags : 'Chromatographie  Planaire'  Biosurfactant  'Ions  métaux  transition'  Souillure  Cellulose Index. décimale : 668.1 Agents tensioactifs : savons, détergents Résumé : Sodium deoxycholate (a biosurfactant) in planar chromatography has been used to investigate the separation and migration behavior of transition metal ions. The chromatographic system comprised of soil-cellulose (3:7, w/w) as stationary phase and mixed micellar solution (sodium deoxycholate-sodium dodecyl sulfate, 1.0% each in 1:1 ratio) containing M5-acetonitrile in 3:2 ratio (v/v) was identified as the best mobile phase for separation and migration of transition metal ions. The Rf value for the metals follows the order, Cu(II) (0.15) < Ag(I) (0.57) < Au(III) (0.91) which also happens to be the order of increasing atomic weight of the metal ions in the periodic group. The detection limit of Cu(II), Ag(I), and Au(III) was found to be 0.22, 1.48, and 7.76 μg zone–1 respectively. The proposed method is robust, sensitive, easy, and reproducible. It has been used for successful identification and separation of above mentioned cations in sample matrices. Permalink : https://e-campus.itech.fr/pmb/opac_css/index.php?lvl=notice_display&id=11928 [article]

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Development of a modified test cell for AC impedance testing of coated Al fins / A. Husain in JOURNAL OF COATINGS TECHNOLOGY AND RESEARCH, Vol. 4, N° 3 (09/2007)  

[article]  inJOURNAL OF COATINGS TECHNOLOGY AND RESEARCH > Vol. 4, N° 3 (09/2007) . - p. 317-325 Titre : Development of a modified test cell for AC impedance testing of coated Al fins Type de document : texte imprimé Auteurs : A. Husain, Auteur ; O. Al-Shamali, Auteur ; P. S. Brahme, Auteur Année de publication : 2007 Article en page(s) : p. 317-325 Note générale : Bibliogr. Langues : Américain (ame) Catégories : Spectroscopie d'impédance électrochimique Tags : 'Electrochemical  impedance  spectroscopy  test  cell'  'EIS  conventional  specimen  holders'  Coating  'Flat  thin  sheet  specimen' Index. décimale : 667.9 Revêtements et enduits Résumé : An innovative test-cell arrangement is proposed and examined for electrochemical impedance spectroscopy (EIS) testing of coated thin sheet or foil samples. This arrangement uses a thin layer of medical cotton fabric as a medium containing and transporting 5% sodium chloride solution. This new EIS cell avoids the intervention of edge effect into EIS measurements of painted material. It also avoids the formation of crevice attack experienced at the edges of conventional sample holders or normally under the edge of the masking material. This arrangement is simple and flexible to suit different sizes and shapes of flat panel and foil samples. It can also be used effectively as specimen holders for other than thin sheets. The test cell is also suitable for any electrochemical tests other than impedance measurements. The accelerated results of the EIS present the viability of the EIS test cell to be used as an accelerated nondestructive, repetitive measurement of coated thin metal substrate. DOI : 10.1007/s11998-007-9043-y En ligne : https://link.springer.com/content/pdf/10.1007%2Fs11998-007-9043-y.pdf Format de la ressource électronique : Pdf Permalink : https://e-campus.itech.fr/pmb/opac_css/index.php?lvl=notice_display&id=3647 [article]

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