An acrylic resin retanning agent with a reinforcing effect - Synthesised by hihg solids content microemulsion copolymerization / Wang Xuechuan in JOURNAL OF THE SOCIETY OF LEATHER TECHNOLOGISTS & CHEMISTS (JSLTC), Vol. 89, N° 4 (07-08/2005)  

[article]  inJOURNAL OF THE SOCIETY OF LEATHER TECHNOLOGISTS & CHEMISTS (JSLTC) > Vol. 89, N° 4 (07-08/2005) . - p. 164-168 Titre : An acrylic resin retanning agent with a reinforcing effect - Synthesised by hihg solids content microemulsion copolymerization Type de document : texte imprimé Auteurs : Wang Xuechuan, Auteur ; An Huari, Auteur ; Sun Ming, Auteur ; Luo Yanhong, Auteur ; Feng Jianyan, Auteur Année de publication : 2005 Article en page(s) : p. 164-168 Note générale : Bibliogr. Langues : Anglais (eng) Catégories : Agents de tannage Caractérisation Copolymères en émulsion Croûte (cuir) On entend par "cuir en croûte" des cuirs ayant subi les opérations jusqu'au tannage, à l'exclusion de toute opération de corroyage ou de finissage, mais qui, par opposition aux wet-blue ont été séchés. Cuirs et peaux -- Propriétés mécaniques Cuirs et peaux de porcs Granulométrie laser Haut extrait sec Latex Microémulsions Polyacryliques Polymérisation en émulsion Retannage Tannage organique Wet-blue (tannage) Peau tannée au chrome (le chrome donne une couleur bleue) Index. décimale : 675.2 Préparation du cuir naturel. Tannage Résumé : An acrylic resin nano-size latex whose colloidal particle size was about 20nm and solids content about 25% was prepared by a high solids content semicontinuous microemulsion copolymerization. The experimental product was employed in retanning drop [bottom] splits of pigs aiming to reinforce the leather. The offer of cross-linking agent and functional monomer were varied in the copolymerization experiment and their effect on the reinforcing function was investigated. The effect of colloidal particle size and dosage of nano-size latex on the reinforcing function also was verified. The particle size of the latex was tested with a laser particle size analyzer, and the composition of the copolymer was analyzed by infrared spectrometry. Multifunction material test equipment was used in the physical testing of the retanned leather. The result of the experiment showed: when the dosage of divinylbenzene (DVB) was 1.2% and the dosage of acrylic acid (AA) 0.8%, the reinforcing performance was the highest. When the colloidal particle size decreased from 64.2nm to 16.3nm, the reinforcing effect was also enhanced. The tensile strength increased by 68%, and the tear strength improved 44% after the drop splits of pigs were retanned with 2% acrylic resin nano-size latex (with respect to the shaved wet blue weight). The effect of the dosage of sodium lauryl sulphate (SLS), n-pentanol (PA), ammonium persulfate (ASP) and AA on the colloidal particle size was also studied. Note de contenu : - EXPERIMENTAL DETAILS : Materials - Synthesis - APPLICATION OF NANO-SIZE LATEX IN RETANNING CHROME TANNED PIG DROP SPLITS : Characterization - RESULTS AND DISCUSSION : Colloidal particle size of the microemulsion copolymer - The IR spectra of BA/MMA/DVB copolymers prepared by microemulsion copolymerization - The effect of functional monomer on the reinforcing function - The effect of cross-linking agent on the reinforcing function - The effect of colloidal particle size on the reinforcing function - The relationship between dosage of retanning agent and reinforcing effect - Table 1 : Recipes used in the series of experiments and average particle size of synthesized latexes - Table 2 : Process details for the retanning applications of nano-size latex on wet blue pig drop splits En ligne : https://drive.google.com/file/d/1GoIENUWkqhu85g-LTxdP-0cZzXD-IvPo/view?usp=share [...] Format de la ressource électronique : Pdf Permalink : https://e-campus.itech.fr/pmb/opac_css/index.php?lvl=notice_display&id=39249 [article]

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Effect of an amphoteric chromium-free polymer retanning agent with reactive aldehyde groups on collagen fibers / Wang Xuechuan in JOURNAL OF THE AMERICAN LEATHER CHEMISTS ASSOCIATION (JALCA), Vol. CXIV, N° 10 (10/2019)  

[article]  inJOURNAL OF THE AMERICAN LEATHER CHEMISTS ASSOCIATION (JALCA) > Vol. CXIV, N° 10 (10/2019) . - p. 373-381 Titre : Effect of an amphoteric chromium-free polymer retanning agent with reactive aldehyde groups on collagen fibers Type de document : texte imprimé Auteurs : Wang Xuechuan, Auteur ; Hao Dongyan, Auteur ; Xiaoye Chai, Auteur ; Li Ji, Auteur Année de publication : 2019 Article en page(s) : p. 373-381 Note générale : Bibliogr. Langues : Américain (ame) Catégories : Absorption Agents de tannage Aldéhydes Un aldéhyde est un composé organique, faisant partie de la famille des composés carbonylés, dont l'un des atomes de carbone primaire (relié au plus à 1 atome de carbone) de la chaîne carbonée porte un groupement carbonyle. L'aldéhyde le plus simple est le formaldéhyde (ou méthanal), aussi appelé formol lorsqu'il est en solution aqueuse. Un aldéhyde dérive formellement d'un alcool primaire (oxydation) dont le groupement hydroxyde -OH est en bout de chaîne et se forme suite à l'enlèvement de deux atomes H d'où le nom "alcool déshydrogéné" ou aldéhyde. Caractérisation Chimie analytique Colorants acides Composés amphotériques Composés organiques -- Synthèse Croûte (cuir) On entend par "cuir en croûte" des cuirs ayant subi les opérations jusqu'au tannage, à l'exclusion de toute opération de corroyage ou de finissage, mais qui, par opposition aux wet-blue ont été séchés. Cuirs et peaux -- Teinture Cuirs et peaux de moutons Douceur (toucher) Essais de résilience Essais dynamiques Frottements (mécanique) Huiles et graisses -- Absorption Liaisons chimiques Polymères Retannage Tannage végétal Température de retrait Index. décimale : 675.2 Préparation du cuir naturel. Tannage Résumé : A chromium-free amphoteric polymer retanning agent was prepared by free radical polymerization reaction of undecylenic aldehyde (UAL), acrylic acid (AA) and dimethyl diallyl ammonium chloride (DADMAC) as raw materials. The structure of amphoteric polymer retanning agent was characterized by FT-IR and 1H-NMR. Amphoteric polymer retanning agent was applied to the retanning of vegetable-tanned light leather to investigate the binding ability of crust leather to anionic dyes, fat liquoring agent and physical-mechanical properties of the crust leather. The results showed that the synthesized amphoteric polymer retanning agent was successfully prepared. The application trial indicated that the amphoteric polymer retanning agent can improve the binding capacity between leather and anion dye and fat liquoring agent in the retanning process. The dye absorption rate of the crust leather was up to 99.58% and the dyeing liquor was clear. Furthermore, color of the crust leather was uniform and full and its K/S value and drywet rub fastness, thickening rate and physical-mechanical properties were higher than that of the retanned leather by acrylic resin retanning agent. In addition, the crust leather after retanning with amphoteric polymer retanning agent has good softness, and the absorption rate of fat liquoring agent was 99.62%. The above results showed that amphoteric polymer retanning agent possessed the good retanning property in vegetable tanned sheep garment leather. Note de contenu : - EXPERIMENTAL : Materials - Instruments - Synthesis of amphoteric polymer retanning agent (PADU) - Fourier Transform Infrared Spectroscopy (FT-IR) - Nuclear Magnetic Resonance Hydgogen Spectra (H-NMR) - Test of shrinkage temperature - Test of uptake of dye - Test of color strength (K/S) value - Test of dry and wet rub fastness - Test of absorption of fat liquoring agent - Test of softness - Test of thickening percentage - Test of tensile strength and tearing strength - SEM observation - RESULTS AND DISCUSSION : FT-IR analysis - H-NMR analysis - Shrinkage - Contrast of bath before and after dyeing - Comparison of pictures of crust leathers retanned by different retanning agent - Dyeing properties of the crust leathers - Comparison of uptakes of fat liquoring agent in different crust leathers - Physical properties of crust leather - SEM observation En ligne : https://drive.google.com/file/d/1ZhR1F8pIPUy_fgU3qYJV6V4qs6tezhHl/view?usp=drive [...] Format de la ressource électronique : Pdf Permalink : https://e-campus.itech.fr/pmb/opac_css/index.php?lvl=notice_display&id=33033 [article]

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Effect of hydrophilic chain extenders on properties of hyperbranched waterborne polyurethane / Wang Xuechuan in JOURNAL OF THE SOCIETY OF LEATHER TECHNOLOGISTS & CHEMISTS (JSLTC), Vol. 100, N° 2 (03-04/2016)  

[article]  inJOURNAL OF THE SOCIETY OF LEATHER TECHNOLOGISTS & CHEMISTS (JSLTC) > Vol. 100, N° 2 (03-04/2016) . - p. 62-66 Titre : Effect of hydrophilic chain extenders on properties of hyperbranched waterborne polyurethane Type de document : texte imprimé Auteurs : Wang Xuechuan, Auteur ; Ren Jing, Auteur ; Qiang Taotao, Auteur Année de publication : 2016 Article en page(s) : p. 62-66 Note générale : Bibliogr. Langues : Anglais (eng) Catégories : Composés organiques -- Synthèse Cuirs et peaux -- Finition Diméthyl butanoïque, Acide Essais de résilience Essais dynamiques Mouillabilité Polymères -- Analyse Polymères -- Propriétés mécaniques Polymères en émulsion Polymères ramifiés Polyuréthanes Propionique diméthylol, Acide Résistance chimique Résistance thermique Index. décimale : 675 Technologie du cuir et de la fourrure Résumé : Using hydroxyl terminated hyperbranched polymer as the core, dimethylol propionic acid (DMPA), dimethylolbutanoic acid (DMBA), carboxylic acid type monomer (DMCA) as the hydrophilic chain extenders respectively, three different types of hyperbranched waterborne polyurethane leather finishing agents were synthesized. The structures and properties of the products were characterized by FT-IR, SEM, AFM and TG. Simultaneously, the mechanical properties, surface wettability and water and solvent resistance of three films were studied. The results found the order of crystallinity to be : DMBA-HWPU Note de contenu : - EXPERIMENTAL PROCEDURES : Materials - Sources - The synthesis of DMCA - The synthesis of hyperbranched waterborne polyurethane - RESULTS AND DISCUSSION : Fourier transforms infrared spectroscopy - X-ray diffraction - Scanning electron microscopy (SEM) - Atomic force microscope (AFM) - Emulsion particle size - Simultaneous thermal analysis curves - Physical and mechanical properties En ligne : https://drive.google.com/file/d/1GQlPV_HUIq7F-tUUWLvt_sE5TcVb2FzQ/view?usp=drive [...] Permalink : https://e-campus.itech.fr/pmb/opac_css/index.php?lvl=notice_display&id=26088 [article]

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Hyperbranched-linear polymers as promising leather additives / Wang Xuechuan in JOURNAL OF THE SOCIETY OF LEATHER TECHNOLOGISTS & CHEMISTS (JSLTC), Vol. 101, N° 1 (01-02/2017)  

[article]  inJOURNAL OF THE SOCIETY OF LEATHER TECHNOLOGISTS & CHEMISTS (JSLTC) > Vol. 101, N° 1 (01-02/2017) . - p. 6-9 Titre : Hyperbranched-linear polymers as promising leather additives Type de document : texte imprimé Auteurs : Wang Xuechuan, Auteur ; Lu Weina, Auteur ; Li Yang, Auteur ; Wang Haijun, Auteur Année de publication : 2017 Article en page(s) : p. 6-9 Note générale : Bibliogr. Langues : Anglais (eng) Catégories : Additifs Caractérisation Cuirs et peaux -- Propriétés mécaniques Groupe hydroxyle Polyesters Polymères -- Synthèse Polymères ramifiés Index. décimale : 675 Technologie du cuir et de la fourrure Résumé : A series of coconut oil-based hydroxyl-terminated hyperbranched-linear polyesters of generations 1-3 (CHBPs) were synthesized using a one-pot method and utilized in leather making. The effect of hyperbranched polymers on collagen fibres was discussed by comparing with linear products at macro level. The experimental results showed that hyperbranched polymers are less lubricating than linear compounds but have more filling abilities. Thickening rates of the leather treated by CHBPs decreased with growing generations due to their hydroxyl groups external to the molecule which will cross-link collagen fibres. In addition, CHBPs at higher generations can shrink location difference sharply. Unluckily, except for CHBP, other products didn't improve the mechanical properties of the leather remarkably. Still, hyperbranched polymers showed great potential application in the leather industry. Note de contenu : - EXPERIMENTAL SECTION : Materials - Synthesis of coconut oil-based hyperbranched polyesters (CHBPs) - Fatliquor process - Characterisation - RESULTS AND DISCUSSION : Synthesis of CHBPs - Filing properties - Solftness properties - Mechanical properties En ligne : https://drive.google.com/file/d/13rfI0LehgtbJN0f0dUMxRZGbzRGbruPM/view?usp=drive [...] Format de la ressource électronique : Pdf Permalink : https://e-campus.itech.fr/pmb/opac_css/index.php?lvl=notice_display&id=27935 [article]

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Hyperbranched polymer polyols : their preparation, modification and use in the leather industry / Wang Xuechuan in JOURNAL OF THE SOCIETY OF LEATHER TECHNOLOGISTS & CHEMISTS (JSLTC), Vol. 93, N° 2 (03-04/2009)  

[article]  inJOURNAL OF THE SOCIETY OF LEATHER TECHNOLOGISTS & CHEMISTS (JSLTC) > Vol. 93, N° 2 (03-04/2009) . - p. 61-72 Titre : Hyperbranched polymer polyols : their preparation, modification and use in the leather industry Type de document : texte imprimé Auteurs : Wang Xuechuan, Auteur ; Yuan Xuzheng, Auteur ; Qiang Taotao, Auteur ; Ren Longfang, Auteur Année de publication : 2009 Article en page(s) : p. 61-72 Note générale : Bibliogr. Langues : Anglais (eng) Index. décimale : 675 Technologie du cuir et de la fourrure Résumé : A series of hyperbranched (poly(amine-ester) polyols (HPAEPs) were synthesized by the polycondensation of N,N-diethylol-3-amine-methylpropionate [prepared by the Michael addition reaction of methyl acrylate (MA) with diethanolamine (DEA)] as an AB2-type monomer with trimethylol propane (TMP) as the core moiety, proceeding in one-step procedure in the melt with p-toluenesulfonic acid (p-TSA) as catalyst. Then, it was modified by diethyl malonate (DEM) in the presence of catalyst (anhydrous K2CO3) via transesterification to obtain a water-soluble hyperbranched polymer with active methylene (HPAM), which can be used as formaldehyde elimination agent. The obtained polymers were characterized by FTIR and TGA. the application results show that HPAEP can be used as the retanning agent with reinforcing performance (tear strength increased by 23.3 % and tensile strength increased by 11.3 %) and bleaching efect (whiteness value increase by 19.8 %) meanwhile. The removal efficiency of free-formaldehyde in leather could reach 56.25 % at 2 % dosage of HPAM for capturing 5h. En ligne : https://drive.google.com/file/d/12Z2LzH5ZpratMjYdV_Cs8EhKwA1PLKpP/view?usp=drive [...] Format de la ressource électronique : Pdf Permalink : https://e-campus.itech.fr/pmb/opac_css/index.php?lvl=notice_display&id=5094 [article]

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Leather retanning performance of carboxylated collagen fibres containing adsorbed Cr(III) / Qiang Taotao in JOURNAL OF THE SOCIETY OF LEATHER TECHNOLOGISTS & CHEMISTS (JSLTC), Vol. 102, N° 4 (07-08/2018)  

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Leather solid waste : a review. A low cost adsorption material based on collagen fibre / Qiang Taotao in JOURNAL OF THE SOCIETY OF LEATHER TECHNOLOGISTS & CHEMISTS (JSLTC), Vol. 100, N° 3 (05-06/2016)  

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Nonparametric bootstrap method for estimating the upper confidence limits of exposure point concentrations of formaldehyde in fur products - A case study of tongxiang city, China / Yuan Xuzheng in JOURNAL OF THE AMERICAN LEATHER CHEMISTS ASSOCIATION (JALCA), Vol. CXII, N° 11 (11/2017)  

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Preparation and application of collagen-based waterborne polyurethane retanning agent / Li Chengtao in JOURNAL OF THE SOCIETY OF LEATHER TECHNOLOGISTS & CHEMISTS (JSLTC), Vol. 101, N° 3 (05-06/2017)  

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Preparation and characterization of collagen grafted by styrene-butyl acrylate and its application for paper sizing / Sufeng Zhang in JOURNAL OF THE AMERICAN LEATHER CHEMISTS ASSOCIATION (JALCA), Vol. CIX, N° 12 (12/2014)  

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Preparation and characterization of modified protein retanning agent based on leather waste / Wang Xuechuan in JOURNAL OF THE SOCIETY OF LEATHER TECHNOLOGISTS & CHEMISTS (JSLTC), Vol. 100, N° 3 (05-06/2016)  

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Progress of application and chemical modification of biomass collagen : a review / Wang Xuechuan in JOURNAL OF THE SOCIETY OF LEATHER TECHNOLOGISTS & CHEMISTS (JSLTC), Vol. 99, N° 5 (09-10/2015)  

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Properties of epoxy modified starch tanning agent combined with aluminum salt / Hao Dongyan in JOURNAL OF THE SOCIETY OF LEATHER TECHNOLOGISTS & CHEMISTS (JSLTC), Vol. 108, N° 1 (01-02/2024)  

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Recycling of raw materials (collagen protein) in the leather industry -high value added application of leather solid waste / Li Chengtao in JOURNAL OF THE SOCIETY OF LEATHER TECHNOLOGISTS & CHEMISTS (JSLTC), Vol. 101, N° 5 (09-10/2017)  

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Research on formaldehycle emission characteristics of leather with porous structure by sealed jar method / Yuan Xuzheng in JOURNAL OF THE SOCIETY OF LEATHER TECHNOLOGISTS & CHEMISTS (JSLTC), Vol. 101, N° 6 (11-12/2017)  

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Synthesis and application of a novel cationic surfactant based on quaternary ammonium salt for leather fatliquoring / Hao Dongyan in JOURNAL OF THE SOCIETY OF LEATHER TECHNOLOGISTS & CHEMISTS (JSLTC), Vol. 103, N° 4 (07-08/2019)  

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Synthesis and evaluation of a novel shavings-based cationic flocculant / Dai Chunji in JOURNAL OF THE SOCIETY OF LEATHER TECHNOLOGISTS & CHEMISTS (JSLTC), Vol. 102, N° 2 (03-04/2018)  

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Synthesis of hyper-branched polymer with terminal amidogen and its application as formaldehyde scavenger in leather / Wang Xuechuan in JOURNAL OF THE AMERICAN LEATHER CHEMISTS ASSOCIATION (JALCA), Vol. CIII, N° 12 (12/2008)  

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Synthesis of ionic liquid-based amphiphilic polymer surfactant and its application in leather fatliquoring / Hao Dongyan in JOURNAL OF THE SOCIETY OF LEATHER TECHNOLOGISTS & CHEMISTS (JSLTC), Vol. 107, N° 2 (03-04/2023)  

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Tanning technique of Crocodylus Niloticus bag leather / Qiang Taotao in JOURNAL OF THE SOCIETY OF LEATHER TECHNOLOGISTS & CHEMISTS (JSLTC), Vol. 99, N° 6 (11-12/2015)  

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