| Titre : |
Fabrication of poly vinyl acetate (PVAc) nanofibers using DMAC solvent : Effect of molecular weight, optimization by Taguchi DoE |
| Type de document : |
texte imprimé |
| Auteurs : |
S. Khanzadeh Borjak, Auteur ; Roohollah Rafee, Auteur ; M. S. Valipour, Auteur |
| Année de publication : |
2020 |
| Article en page(s) : |
p. 257-267 |
| Note générale : |
Bibliogr. |
| Langues : |
Anglais (eng) |
| Catégories : |
Diméthylacétamide
Electrofilature
Morphologie (matériaux)
Nanofibres
Plan d'expérience
Poids moléculaires
Polyacétate de vinyle
Sol-gel, Procédé
Taguchi, Méthodes de (Contrôle de qualité)
|
| Index. décimale : |
668.4 Plastiques, vinyles |
| Résumé : |
This study experimentally investigated the effect of different molecular weights of Poly vinyl acetate (PVAc) on electrospinning ability of PVAc/DMAC sol-gels. The influences of polymer solution concentration and electrospinning process parameters (needle tip to collector distance, flow rate, and applied voltage) on the mean diameters of electrospun PVAc nanofibers were examined by design of the experiments based on the Taguchi method. Three levels were considered for each process factor as inputs for the Taguchi DoE technique. To characterize and optimize the mentioned parameters, Taguchi's L9 orthogonal design (four parameters, three levels) was used. The "smaller-the-better" approach was used to utilize the optimum production conditions based on the signal-to-noise (S/N) ratios. The results indicated that the polymer solution concentration was the most important parameter on the mean diameter of the nanofibers. The minimum nanofiber diameter at the optimum conditions was measured about 52 nm. In conclusion, the Taguchi DoE method was identified as an efficient technique to characterize and optimize the electrospinning process parameters to increase the robustness of nanofiber fabrication. |
| Note de contenu : |
- Effect of PVAc molecular weigh on electrospinning
- Nanofiber morphology and diameter (Taguchi DoE)
- Effect of flow rate on fiber diameter
- Effect of TCD on fiber diameter
- Effect of aplied voltage on fiber diameter
- Effect of solution concentration on fiber diameter
- Confirmation of Taguchi Design of Experiments |
| DOI : |
https://doi.org/10.3139/217.3920 |
| En ligne : |
https://drive.google.com/file/d/1CQ6GJ0TPFSaogTPZ0scFjTVkHEz8D4Fw/view?usp=drive [...] |
| Format de la ressource électronique : |
Pdf |
| Permalink : |
https://e-campus.itech.fr/pmb/opac_css/index.php?lvl=notice_display&id=34492 |
in INTERNATIONAL POLYMER PROCESSING > Vol. XXXV, N° 3 (07/2020) . - p. 257-267
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Fabrication of poly vinyl acetate (PVAc) nanofibers using DMAC solvent : Effect of molecular weight, optimization by Taguchi DoE in INTERNATIONAL POLYMER PROCESSING, Vol. XXXV, N° 3 (07/2020)
