[article]
| Titre : |
Synthesis and characterization of mesoporous alumina-zirconia as catalyst support for suzuki coupling reaction |
| Type de document : |
texte imprimé |
| Auteurs : |
J. Ji, Auteur ; K. Zhang, Auteur ; Y. Qin, Auteur ; Y. Kong, Auteur ; S. Li, Auteur ; Y. Wang, Auteur |
| Année de publication : |
2012 |
| Article en page(s) : |
p. 43-47 |
| Note générale : |
Bibliogr. |
| Langues : |
Anglais (eng) |
| Catégories : |
Alumine
Caractérisation
Composés inorganiques -- Synthèse
Copolymères séquencés
Matériaux mésoporeux
Réaction de couplage
Surfactants
Zirconium
|
| Index. décimale : |
668.1 Agents tensioactifs : savons, détergents |
| Résumé : |
One pot facile synthesis of ordered mesoporous alumina-supported zirconia with high thermal stability and large pore sizes by evaporation-induced method was systematically investigated. The strategy based on a sol-gel process associated with nonionic triblock copolymers PPO-PEO-PPO as templates in ethanolic solution. Small-angle XRD, TEM, and nitrogen adsorption and desorption results showed that these composites possessed an ordered 2D hexagonal mesostructure, resisted to high temperature up to 1000°C, and had large surface areas and narrow poresize distributions. Loaded with palladium, the mesoporous alumina-zirconia composite exhibited high catalytic activity in Suzuki coupling of 2-bromotoluene with phenylboronic acid. |
| Note de contenu : |
- EXPERIMENTAL : Materials - Synthesis - Characterizations
- RESULTS AND DISCUSSION : Preparation and characterization of mesoporous Al2O3-ZRO2 supports - Catalysis activity of Pd/Al2O3-ZRO2 catalyst |
| Permalink : |
https://e-campus.itech.fr/pmb/opac_css/index.php?lvl=notice_display&id=13323 |
in TENSIDE, SURFACTANTS, DETERGENTS > Vol. 49, N° 1 (01-02/2012) . - p. 43-47
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Synthesis and characterization of mesoporous alumina-zirconia as catalyst support for suzuki coupling reaction in TENSIDE, SURFACTANTS, DETERGENTS, Vol. 49, N° 1 (01-02/2012)
