Fabrication of poly vinyl acetate (PVAc) nanofibers using DMAC solvent : Effect of molecular weight, optimization by Taguchi DoE / S. Khanzadeh Borjak in INTERNATIONAL POLYMER PROCESSING, Vol. XXXV, N° 3 (07/2020)  

[article]  inINTERNATIONAL POLYMER PROCESSING > Vol. XXXV, N° 3 (07/2020) . - p. 257-267 Titre : Fabrication of poly vinyl acetate (PVAc) nanofibers using DMAC solvent : Effect of molecular weight, optimization by Taguchi DoE Type de document : texte imprimé Auteurs : S. Khanzadeh Borjak, Auteur ; Roohollah Rafee, Auteur ; M. S. Valipour, Auteur Année de publication : 2020 Article en page(s) : p. 257-267 Note générale : Bibliogr. Langues : Anglais (eng) Catégories : Diméthylacétamide Electrofilature Morphologie (matériaux) Nanofibres Plan d'expérience Poids moléculaires Polyacétate de vinyle Sol-gel, Procédé Taguchi, Méthodes de (Contrôle de qualité) Index. décimale : 668.4 Plastiques, vinyles Résumé : This study experimentally investigated the effect of different molecular weights of Poly vinyl acetate (PVAc) on electrospinning ability of PVAc/DMAC sol-gels. The influences of polymer solution concentration and electrospinning process parameters (needle tip to collector distance, flow rate, and applied voltage) on the mean diameters of electrospun PVAc nanofibers were examined by design of the experiments based on the Taguchi method. Three levels were considered for each process factor as inputs for the Taguchi DoE technique. To characterize and optimize the mentioned parameters, Taguchi's L9 orthogonal design (four parameters, three levels) was used. The "smaller-the-better" approach was used to utilize the optimum production conditions based on the signal-to-noise (S/N) ratios. The results indicated that the polymer solution concentration was the most important parameter on the mean diameter of the nanofibers. The minimum nanofiber diameter at the optimum conditions was measured about 52 nm. In conclusion, the Taguchi DoE method was identified as an efficient technique to characterize and optimize the electrospinning process parameters to increase the robustness of nanofiber fabrication. Note de contenu : - Effect of PVAc molecular weigh on electrospinning - Nanofiber morphology and diameter (Taguchi DoE) - Effect of flow rate on fiber diameter - Effect of TCD on fiber diameter - Effect of aplied voltage on fiber diameter - Effect of solution concentration on fiber diameter - Confirmation of Taguchi Design of Experiments DOI : https://doi.org/10.3139/217.3920 En ligne : https://drive.google.com/file/d/1CQ6GJ0TPFSaogTPZ0scFjTVkHEz8D4Fw/view?usp=drive [...] Format de la ressource électronique : Pdf Permalink : https://e-campus.itech.fr/pmb/opac_css/index.php?lvl=notice_display&id=34492 [article]

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Processing of polyetherimide/cloisite 30B nanocomposite by vibration casting method / M. Dwivedi in INTERNATIONAL POLYMER PROCESSING, Vol. XXIX, N° 5 (11/2014)  

[article]  inINTERNATIONAL POLYMER PROCESSING > Vol. XXIX, N° 5 (11/2014) . - p. 635-640 Titre : Processing of polyetherimide/cloisite 30B nanocomposite by vibration casting method Type de document : texte imprimé Auteurs : M. Dwivedi, Auteur ; K. K. Gaur, Auteur ; S. Alam, Auteur ; Naresh Bhatnagar, Auteur ; A. K. Ghosh, Auteur Année de publication : 2014 Article en page(s) : p. 635-640 Note générale : Bibliogr. Langues : Anglais (eng) Catégories : Cloisite Diméthylacétamide Matériaux hybrides -- Propriétés thermomécaniques Polyéther imide Vibrations (mécanique) Index. décimale : 668.9 Polymères Résumé : Vibration casting method was developed for making polyetherimide (PEI)/Cloisite 30B nanocomposite. Towards this, a vibration casting apparatus was designed and developed. Vibration casting apparatus provided vibrational energy and heat, simultaneously. The processing parameters were established for vibration casting in terms of frequency of vibration, temperature, time and viscosity of casting mixture. Casting mixture of PEI/Cloisite 30B/N,N-dimethyl acetamide (DMAc) was made by dissolving PEI in DMAc and then mixing Cloisite 30B in this solution. The viscosity of PEI/Cloisite 30B/DMAc mixture was optimized for casting by controlling the volume fraction of PEI in DMAc. Morphology of PEI/Cloisite 30B nanocomposite was examined by wide angle X-ray diffraction, transmission electron microscopy, scanning electron microscopy and contact angle measurement. Mechanical and thermal properties of PEI/Cloisite 30B nanocomposite were also compared with that of neat PEI to ascertain the efficacy of vibration casting method. Note de contenu : - EXPERIMENTAL : 1. Materials - 2. Design and Development of Vibration Casting Apparatus - 3. Optimisation of Viscosity - 4. Estimation of Frequency - 5. Processing of PEI/Cloisite 30B Nanocomposite - 6. Evaluation of Morphology - 7. Evaluation of Mechanical and Thermal Properties - RESULTS AND DISCUSSION : 1. Optimisation of Viscosity for Casting Mixture - 2. Frequency of Vibration to Cast PNC Film - 3. Morphology - 4. Mechanical and Thermal Properties DOI : 10.3139/217.2952 En ligne : https://drive.google.com/file/d/13ZlgK1wxyMJJC5UIE9yB6Xk1I2VR7oRr/view?usp=drive [...] Format de la ressource électronique : Pdf Permalink : https://e-campus.itech.fr/pmb/opac_css/index.php?lvl=notice_display&id=22243 [article]

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