Titre : |
Analysis of the composition of masked aluminium complexes by HPLC combined with capillary electrophoresis |
Type de document : |
texte imprimé |
Auteurs : |
Eisuke Takata, Auteur ; Yoshimichi Maeda, Auteur ; Yasuhiro Ishii, Auteur ; Kunio Shirai, Auteur |
Année de publication : |
1994 |
Article en page(s) : |
p. 89-97 |
Note générale : |
Bibliogr. |
Langues : |
Américain (ame) |
Index. décimale : |
675 Technologie du cuir et de la fourrure |
Résumé : |
Size-exclusion, high performance liquid chromatography (HPLC) combined with capillary electrophoresis was applied to analyze the composition of oxycarboxylate-masked aluminium complexes. Using a HPLC column (asahipak GS-220) connected to a refractive index detector, oxycarboxylate-masked aluminium complexes were separated into several peak fractions.Oxy-acid content of the fractions was successfully determined by capillary electrophoresis (shimadzu IP-2A). Glycolate- and lactate-masked aluminium complexes contained the major portion of the components to be eluted in the lower molecular size region while a considerable portion of tartrate- and citrate-masked complexes eluted in the higher molecular size region. All masked-aluminium fractions contained oxy-acids at an equivalent-to-mole of al ratio of 0.1 to 0.2. |
En ligne : |
https://drive.google.com/file/d/1v7GVZYDcPFjZMw_8r84MDrpAgTwkSg3l/view?usp=drive [...] |
Format de la ressource électronique : |
Pdf |
Permalink : |
https://e-campus.itech.fr/pmb/opac_css/index.php?lvl=notice_display&id=8081 |
in JOURNAL OF THE AMERICAN LEATHER CHEMISTS ASSOCIATION (JALCA) > Vol. LXXXIX, N° 4 (04/1994) . - p. 89-97