Study on the degreasing of sheep skin using subcritical fluid extraction / Qiao Xia in JOURNAL OF THE AMERICAN LEATHER CHEMISTS ASSOCIATION (JALCA), Vol. CXVI, N° 2 (02/2021)  

[article]  inJOURNAL OF THE AMERICAN LEATHER CHEMISTS ASSOCIATION (JALCA) > Vol. CXVI, N° 2 (02/2021) . - p. 39-45 Titre : Study on the degreasing of sheep skin using subcritical fluid extraction Type de document : texte imprimé Auteurs : Qiao Xia, Auteur ; Zhang Meina, Auteur ; Bo Mao, Auteur ; Hong Dai, Auteur ; Zongcai Zhang, Auteur Année de publication : 2021 Article en page(s) : p. 39-45 Note générale : Bibliogr. Langues : Américain (ame) Catégories : Caractérisation Cuirs et peaux -- Analyse Cuirs et peaux -- Dégraissage Cuirs et peaux de moutons Extraction (chimie) Peau -- Histologie Peaux brutes Pentane Le pentane est un alcane linéaire de formule C5H12. Le terme pentane désigne aussi par extension abusive17 les trois isomères C5H12 : le n-pentane, le 2-méthylbutane ou isopentane et le 2,2-diméthylpropane ou néopentane. Ces diverses molécules comportent toutes cinq atomes de carbone. Utilisations : Le pentane est un solvant couramment utilisé en chimie organique. Propriétés chimiques : Le pentane brûle dans l'air selon la réaction : C5H12 + 8O2 —> 5CO2 + 6H2O (Wikipedia) Index. décimale : 675 Technologie du cuir et de la fourrure Résumé : Degreasing is one of the important processes for the production of leather and fur. This study aimed to develop a degreasing method using subcritical n-pentane. Sheep skin was chosen as raw skin for this investigation. The best possible combination of degreasing parameters was found using single factor experiment and response surface methodology. The effects of temperature and pressure on the degreasing efficiency were evaluated further with histological analysis. The results showed that the optimum degreasing parameters were a degreasing time of 58 min, pressure of 0.45 MPa, temperature of 41.0°C and thus yielded a degreasing rate of 52.46％ theoretically and 51.46% experimentally. Histological sections showed that the degreasing effect of subcritical n-pentane was quite significant and the lipid droplets around the hair follicles were dramatically reduced. It has been proven that subcritical n-pentane degreasing is an effective technique for sheep skin degreasing. Note de contenu : - EXPERIMENTAL : Materials & instruments - Experiment procedure - Sample preparation - Degreasing with subcritical n-pentane extraction - Single factor experiment design of subcritical n-pentane degreasing process - Optimization design of subcritical n-pentane degreasing process by RSM - Characterization of degreasing effect - Histological analysis of degreased skin - RESULTS AND DISCUSSION : Effect of degreasing - Table 1 : Single factor experiment scheme - Table 2 : Factor table for single factor experiment - Table 3 : Response surface experiment level and coding - Table 4 : Experimental scheme of response surface methodology and response value of degreasing rate - Table 5 : Analysis of variance of regression model of subcritical n-pentane degreasing - Fig. 1 : The sheep skin degreasing procedure with subcritical n-pentane - Fig. 2 : Single factor results - Fig. 3 : Residuals - Fig. 4 : Response surface graph and contour map - Fig. 5 : Histological photomicrographs of degreased skin under different temeprature - Fig. 6 : Histological photomicrographs of degreasing skin under different pressure DOI : https://doi.org/10.34314/jalca.v116i2.4234 En ligne : https://drive.google.com/file/d/1fFEfsYfERS70jjgP-KtN7vOTfnm400QO/view?usp=drive [...] Format de la ressource électronique : Pdf Permalink : https://e-campus.itech.fr/pmb/opac_css/index.php?lvl=notice_display&id=35307 [article]

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