| Titre : |
Synthesis of Fe3O4 nanoparticles with tunable sizes for the removal of Cr(VI) from aqueous solution |
| Type de document : |
texte imprimé |
| Auteurs : |
Yibing Feng, Auteur ; Yi Du, Auteur ; Zhongtao Chen ; Minxing Du ; Kai Yang ; Xingjie Lv ; Zhongfu Li |
| Année de publication : |
2018 |
| Article en page(s) : |
p. 1145-1155 |
| Note générale : |
Bibliogr. |
| Langues : |
Américain (ame) |
| Catégories : |
Absorbants et adsorbants
Adsorption
Caractérisation
Chrome hexavalent
Déchets industriels -- Elimination
Nanoparticules
Nanoparticules -- Synthèse
Oxyde de fer
Solutions aqueuses (chimie)
Triéthanolamine
|
| Index. décimale : |
667.9 Revêtements et enduits |
| Résumé : |
In this study, size-tunable magnetite (Fe3O4) nanocrystal spheres were promptly synthesized by a facile one-pot solvothermal process with the presence of triethanolamine as an additive. The as-synthesized Fe3O4 nanoparticles were characterized by X-ray diffraction, transmission electron microscopy, scanning electron microscopy, Fourier-transform infrared spectroscopy, and vibrating sample magnetometer. The results showed that the synthesized nanoparticles were in the size range of 30–350 nm, had well-defined Fe3O4 crystal phase, and had favorable saturation magnetization. The effects of various important parameters, such as initial Cr(VI) concentration, temperature, and pH, on the adsorption properties of the as-obtained Fe3O4 particles for the removal of Cr(VI) in aqueous solution were deeply analyzed and studied. The results confirmed that the adsorption efficiency was highly pH dependent, decreased with the increasing of initial concentration of Cr(VI), and increased with increasing temperature. The adsorption data were well fitted with the Langmuir isotherm. The maximum adsorption capacity calculated from the Langmuir isotherm was 56.625 mg g−1 at temperature of 35°C and pH of 2.0. |
| Note de contenu : |
- EXPERIMENTAL SECTION : Chemicals - Synthesis and characterization of the adsorbent - Adsorption experiments
- RESULTS AND DISCUSSION : Adsorbent characterization - Effect of temperature and contact time - Effect of pH on removal of Cr(VI) ions from aqueous solution and the distribution of Cr(VI) and Cr(III) species in residue solutions - Effect of initial concentration of Cr(VI) and the adsorption isotherms - Adsorption mechanism |
| DOI : |
10.1007/s11998-018-0052-9 |
| En ligne : |
https://link.springer.com/content/pdf/10.1007%2Fs11998-018-0052-9.pdf |
| Format de la ressource électronique : |
Pdf |
| Permalink : |
https://e-campus.itech.fr/pmb/opac_css/index.php?lvl=notice_display&id=31141 |
in JOURNAL OF COATINGS TECHNOLOGY AND RESEARCH > Vol. 15, N° 5 (09/2018) . - p. 1145-1155
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