| Titre : |
Application of nickel-catalysed reduction and azo dye reactions for the determination of tinidazole |
| Type de document : |
texte imprimé |
| Auteurs : |
A. V. S. S. Prasad, Auteur ; P. Murhalidhar Reddy, Auteur ; K. Shanker, Auteur ; R. Rohini, Auteur ; V. Ravinder, Auteur |
| Année de publication : |
2009 |
| Article en page(s) : |
p. 284-287 |
| Note générale : |
Bibliogr. |
| Langues : |
Anglais (eng) |
| Index. décimale : |
667.3 Teinture et impression des tissus |
| Résumé : |
A macrocyclic Schiff base nickel(ii) complex was synthesised via template synthesis by treating acetylacetone with 1,8-diaminonaphthalene in the presence of nickel chloride in a 2:2:1 ratio in an aqueous methanol solution at 75 °C for 30 min. It was characterised by elemental, infrared, proton and carbon nuclear magnetic resonance and mass spectral analysis and used as a catalyst for the reduction of tinidazole. The reduced tinidazole was treated with nitrous acid and 2-naphthol and the resulting azo dye was used for the spectrophotometric determination of the reduction product of tinidazole. |
| DOI : |
10.1111/j.1478-4408.2009.00208.x |
| En ligne : |
http://onlinelibrary.wiley.com/doi/10.1111/j.1478-4408.2009.00208.x/pdf |
| Format de la ressource électronique : |
Pdf |
| Permalink : |
https://e-campus.itech.fr/pmb/opac_css/index.php?lvl=notice_display&id=6864 |
in COLORATION TECHNOLOGY > Vol. 125, N° 5 (2009) . - p. 284-287
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